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Dataset on the comparison of synthesized and commercial zeolites for potential solar adsorption refrigerating system

机译:用于潜在的太阳能吸附制冷系统的合成沸石和商用沸石比较的数据集

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摘要

The purpose of this dataset is to provide a comparison between synthesized and commercial 4A and 13X type zeolites. Metakaolin produced from the calcination of beneficiated kaolin at 750 °C for 4 h was dealuminated using sulphuric acid to get the required silica to alumina ratio for the zeolite synthesis. Zeolite 4A and 13X samples were characterized along-side with the commercial variants using X-ray fluorescence (XRF), X-ray diffraction (XRD), Brunauer, Emmett and Teller (BET) and scanning electron microscopy (SEM) techniques. These analyses revealed that, the zeolites synthesized are of comparatively acceptable quality. The pore size of 120.859 nm, pore volume of 0.0065 cm3/g and surface area of 22 m2/g were obtained from BET analyses for zeolite 4A synthesized from kaolin, while the commercial zeolite 4A used as control gave pore size of 58.143 nm, pore volume of 0.2462 cm3/g and surface area of 559.13 m2/g. In the same vein, the pore size of 10.5059 nm, pore volume of 0.135847 cm3/g and surface area of 324.584 m2/g were obtained from BET analyses for zeolite 13X synthesized from kaolin, while the commercial zeolite 13X gave pore size of 7.2752 nm, pore volume of 0.135951 cm3/g and surface area of 310.0906 m2/g.
机译:该数据集的目的是提供合成4A和商用4A和13X型沸石的比较。用硫酸脱除选矿高岭土在750°C下煅烧4 h所产生的偏高岭土,以得到合成沸石所需的硅铝比。使用X射线荧光(XRF),X射线衍射(XRD),Brunauer,Emmett和Teller(BET)和扫描电子显微镜(SEM)技术,对沸石4A和13X样品以及商用变体进行了表征。这些分析表明,合成的沸石具有相对可接受的质量。通过对高岭土合成的4A沸石进行BET分析,获得孔径为120.859 nm,孔径为0.0065 cm 3 / g和表面积为22 m 2 / g。商业沸石4A的孔径为58.143 nm,孔体积为0.2462 cm 3 / g,比表面积为559.13 m 2 / g。在相同的静脉中,通过沸石的BET分析获得了孔径为10.5059 nm,孔径为0.135847 cm 3 / g和表面积为324.584 m 2 / g 13X由高岭土合成,而商品沸石13X的孔径为7.2752 nm,孔体积为0.135951 cm 3 / g,表面积为310.0906 m 2 / g。

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