Eight gibberellins (GAs) were identified from vegetative shoots of navel orange trees (Citrus sinensis L. Osbeck cv Washington) after sequential purification by reverse-phase C18 high performance liquid chromatography, Nucleosil 5N(CH3)2 high performance liquid chromatography, and capillary gas chromatography-mass spectrometry. GA1, GA17, GA19, GA20, GA29, and iso-GA3 were identified based on the full scan mass spectra and Kovats retention indices. GA8 was tentatively identified based on the comparison of the full scan mass spectra with the published spectra. GA44 was tentatively identified from the characteristic masses at the correct Kovats retention index.
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机译:经反相C18高效液相色谱,Nucleosil 5N(CH3)2高效液相色谱和毛细管气体顺序纯化后,从脐橙树(Citrus sinensis L. Osbeck cv Washington)的营养枝中鉴定出八个赤霉素(GAs)。色谱-质谱联用。 GA1,GA17,GA19,GA20,GA29和iso-GA3是根据全扫描质谱和Kovats保留指数确定的。根据全扫描质谱图与已发布质谱图的比较,初步确定了GA8。初步从特征质量中以正确的科瓦兹保留指数鉴定出GA44。
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