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Solution Based Methods for the Fabrication of Carbon Nanotube Modified Atomic Force Microscopy Probes

机译:基于溶液的碳纳米管修饰原子力显微镜探针的制备方法

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摘要

High aspect ratio carbon nanotubes are ideal candidates to improve the resolution and lifetime of atomic force microscopy (AFM) probes. Here, we present simple methods for the preparation of carbon nanotube modified AFM probes utilising solvent evaporation or dielectrophoresis. Scanning electron microscopy (SEM) of the modified probes shows that the carbon nanotubes attach to the probe apex as fibres and display a high aspect ratio. Many of the probes made in this manner were initially found to exhibit anomalous feedback characteristics during scanning, which rendered them unsuitable for imaging. However, we further developed and demonstrated a simple method to stabilise the carbon nanotube fibres by scanning with high force in tapping mode, which either shortens or straightens the carbon fibre, resulting in stable and high quality imaging AFM imaging.
机译:高纵横比的碳纳米管是提高原子力显微镜(AFM)探针的分辨率和寿命的理想候选者。在这里,我们介绍了利用溶剂蒸发或介电电泳制备碳纳米管修饰的AFM探针的简单方法。改性探针的扫描电子显微镜(SEM)显示,碳纳米管以纤维的形式附着在探针的顶端,并显示出高的长宽比。最初发现以这种方式制成的许多探针在扫描过程中表现出异常的反馈特性,这使其不适用于成像。但是,我们进一步开发并证明了一种简单的方法,可以通过在攻丝模式下用高力扫描来稳定碳纳米管纤维,从而缩短或拉直碳纤维,从而获得稳定且高质量的成像AFM成像。

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