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Defect Creation in the Root of Single-Crystalline Turbine Blades Made of Ni-Based Superalloy

机译:镍基高温合金单晶涡轮叶片根部缺陷的产生

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摘要

An analysis of the defects in the vicinity of the selector–root connection plane occurring during the creation of single-crystalline turbine blades made of CMSX-6 Ni-based superalloy was performed. X-ray diffraction topography, scanning electron microscopy, and positron annihilation lifetime spectroscopy were used. Comparing the area of undisturbed axial growth of dendrites to the area of lateral growth concluded that the low-angle boundaries-like (LAB-like) defects were created in the root as a result of unsteady-state lateral growth of some secondary dendrite arms in layers of the root located directly at the selector–root connection plane. Additional macroscopic low-angle boundaries (LABs) with higher misorientation angles were created as a result of concave curvatures of liquidus isotherm in platform-like regions near selector–root connections. Two kinds of vacancy-type defects, mono-vacancies and vacancy clusters, were determined in relation to the LABs and LAB-like defects. Only mono-vacancies appeared in the areas of undisturbed axial growth. Reasons for the creation of macroscopic LABs and LAB-like defects, and their relationships with vacancy-type defects were discussed.
机译:对在制造由CMSX-6 Ni基高温合金制成的单晶涡轮叶片过程中发生的选择器-根部连接面附近的缺陷进行了分析。使用X射线衍射形貌,扫描电子显微镜和正电子an没寿命谱。比较树枝状晶体未受干扰的轴向生长面积与横向生长的面积,得出的结论是,由于某些次生枝晶臂的非稳态横向生长,在根部产生了低角度边界样(LAB状)缺陷。根的直接位于选择器-根连接平面的层。由于在选择器-根部连接附近的平台状区域中,液相线等温线的凹曲率降低,因此产生了其他较大的宏观低角度边界(LABs),从而产生了较大的取向错误。相对于LAB和类LAB缺陷,确定了两种空位类型缺陷:单空位和空位簇。在轴向生长不受干扰的区域中仅出现单空位。讨论了产生宏观LAB和类LAB缺陷的原因,以及它们与空位型缺陷的关系。

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