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Effect of Heat Curing Method on the Mechanical Strength of Alkali-Activated Slag Mortar after High-Temperature Exposure

机译:高温暴露后热固化方法对碱活化矿渣砂浆机械强度的影响

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摘要

The aim of this work was to study the mechanical strength and microstructure changes of alkali-activated slag mortar (AAS mortar) after being heat treated in the temperature range of 200–1000 °C. The AAS mortar was cured in the ambient condition (20 ± 5 °C, 60 ± 5% RH) (Relative humidity: RH) and high temperature condition (80 °C) for 27 days with three different heating regimes: curing in a dry oven, curing in sealed plastic bags, and in a steam environment. The activator for the AAS synthesis was a mixture of sodium silicate solution (water glass) and sodium hydroxide (NaOH) with a SiO2/Na2O weight ratio of 1, and a dosage of 4% Na2O by slag weight. Thermogravimetric analysis (TGA) and scanning electron microscopy (SEM) incorporated with energy-dispersive X-ray spectroscopy (EDX) were used to assess the mortar microstructure change. The results revealed that the curing method significantly affected the mechanical strength of AAS at temperatures lower than 800 °C. The heat treatment at late age of 28 days was more beneficial for compressive strength enhancement in specimens without using heat curing methods.
机译:这项工作的目的是研究碱活化矿渣砂浆(AAS砂浆)在200–1000°C的温度范围内进行热处理后的机械强度和微观结构变化。 AAS砂浆在环境条件(20±5°C,60±5%RH)(相对湿度:RH)和高温条件(80°C)下用三种不同的加热方式固化27天:在干燥条件下固化烤箱,在密封的塑料袋中固化,并在蒸汽环境中固化。用于AAS合成的活化剂是SiO2 / Na2O重量比为1的硅酸钠溶液(水玻璃)和氢氧化钠(NaOH)的混合物,炉渣重量为4%Na2O。结合了能量色散X射线光谱(EDX)的热重分析(TGA)和扫描电子显微镜(SEM)评估了砂浆的微观结构变化。结果表明,在低于800°C的温度下,固化方法会显着影响AAS的机械强度。在不使用热固化方法的情况下,在28天后期进行热处理对于提高样品的抗压强度更为有利。

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