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The Effect of Exposed Glass Fibers and Particles of Bioactive Glass on the Surface Wettability of Composite Implants

机译:暴露的玻璃纤维和生物活性玻璃颗粒对复合植入物表面润湿性的影响

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摘要

Measurement of the wettability of a material is a predictive index of cytocompatibility. This study was designed to evaluate the effect of exposed E-glass fibers and bioactive glass (BAG) particles on the surface wettability behavior of composite implants. Two different groups were investigated: (a) fiber reinforced composites (FRCs) with different fiber orientations and (b) polymer composites with different wt. % of BAG particles. Photopolymerized and heat postpolymerized composite substrates were made for both groups. The surface wettability, topography, and roughness were analyzed. Equilibrium contact angles were measured using the sessile drop method. Three liquids were used as a probe for surface free energy (SFE) calculations. SFE values were calculated from contact angles obtained on smooth surfaces. The surface with transverse distribution of fibers showed higher (P < 0.001) polar (γ P) and total SFE (γ TOT) components (16.9 and 51.04 mJ/m2, resp.) than the surface with in-plane distribution of fibers (13.77 and 48.27 mJ/m2, resp.). The increase in BAG particle wt. % increased the polar (γ P) value, while the dispersive (γ D) value decreased. Postpolymerization by heat treatment improved the SFE components on all the surfaces investigated (P < 0.001). Composites containing E-glass fibers and BAG particles are hydrophilic materials that show good wettability characteristics.
机译:材料润湿性的测量是细胞相容性的预测指标。本研究旨在评估裸露的电子玻璃纤维和生物活性玻璃(BAG)颗粒对复合植入物表面润湿性行为的影响。研究了两个不同的组:(a)具有不同纤维取向的纤维增强复合材料(FRC)和(b)具有不同wt的聚合物复合材料。 BAG颗粒的百分比。两组均制备了光聚合和热后聚合的复合基材。分析了表面润湿性,形貌和粗糙度。平衡接触角使用无滴法测量。三种液体用作表面自由能(SFE)计算的探针。根据在光滑表面上获得的接触角计算SFE值。具有纤维横向分布的表面显示出较高的(P <0.001)极性(γ P )和总的SFE(γ TOT )组分(16.9和51.04 mJ / m 2 ,分别比具有平面内纤维分布的表面(13.77和48.27 mJ / m 2 ,分别)高。 BAG颗粒重量的增加。 %增加极性(γ P )值,而色散(γ D )值减小。通过热处理进行的后聚合改进了所有研究表面上的SFE成分(P <0.001)。包含电子玻璃纤维和BAG颗粒的复合材料是亲水性材料,具有良好的润湿性。

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