γ-氨丙基三硅氧烷的合成

摘要

以γ-氨丙基二乙氧基甲基硅烷、六甲基二硅氧烷为原料，合成了γ-氨丙基三硅氧烷，用二次蒸馏水除去副产物，产物收率52.4％，并利用核磁共振氢谱（1 H NMR）和红外光谱（IR）对产物结构进行了表征。%γ-aminopropyl trisiloxane was synthesized with 3-aminopropyl methyldiethoxysilane and hexa-methyldisiloxane.By-products were removed by redistilled water with the yield of 52.4%.The product struc-ture was characterized by 1 H NMR and IR.