首页> 中文期刊> 《矿物冶金与材料学报:英文版》 >A new sol-gel process for preparing Ba(Mg_(1/3)Nb_(2/3))O_3 nanopowders

A new sol-gel process for preparing Ba(Mg_(1/3)Nb_(2/3))O_3 nanopowders

         

摘要

Commercially available niobium (V) oxide [Nb2O5], with barium acetate [Ba(CH3COO)2] and magnesium acetate At first, Nb2O5 reacted with melting sodium hydroxide and transformed into dispersible oxide. The resulting glassy substance after cooling was dispersed and washed several times in distilled water to remove the Na+ ions. The as-prepared colloidal Nb2O5.nH2O was subsequently mixed with acetic solution of barium acetate and magnesium acetate according to the required molar proportions and followed by gelation. The ultrafine BMN powders were finally obtained after heat-treating the gel at 820℃ for 1 h, and the assintered nanoceramics revealed a high relative density of 98.2%, and a high microwave Q-factor, of 10397 at 1.45GHz.

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