Rice husk was used to prepare the silica of amorphous nature being several times more reactive than that obtained from the mineral kingdom. Number of rice husk batches were pyroprocessed under varying time-temperature parameters for this purpose. The ash resulting from a batch pyroprocessed at 500℃ for 8 h contained 92.01% silica. It was upgraded to 98.50% by applying physicochemical purification procedures. The mineral, wollastonite (CaSiO3), was synthesized from thus prepared silica and limestone containing 55.91% CaO. Solid state reaction, between CaO and SiO2 was attempted at different temperatures in the presence of a mineralizer. The sintering temperature,for affecting the said synthesis, was ranged between 900℃ to 1300℃ with the steps of 100℃. Specific chemical analysis techniques were applied to determine the effectiveness of carried out reaction and promising batches were subsequently subjected to XRD investigations. The produced mineral was also characterized regarding its physical properties like: colour, hardness, melting point and specific gravity. Percent yield of the produced wollastonite was also estimated and compared with that of obtained by other researchers who synthesized it by using silica from mineral kingdom. Batches sintered at 1200℃ and 1300℃ for 1 h showed the overall best results.
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