采用热压变形法对NdFeB磁体晶间富Nd相的显微组织进行了研究。实验结果表明, NdFeB磁体经真空热压变形后, 富Nd相不再平均地分布在磁体晶间,而是聚集成团块状或从磁体边缘渗出。 显微组织分析表明, 富Nd相主要是由α-Nd和Nd2Fe17两相组成,与Nd-Fe合金的共晶组织成分接近 对于晶间添加Al元素的磁体,Al溶入晶间形成Nd2Fe15Al2相弥散地分布在晶界上, 这有益于磁体矫顽力的提高;对于晶间添加Cu元素的磁体, 晶间没有发现有新相产生%The microstructure of intergranular Nd-rich phase of sintered NdFeB magnets has been studied by means of thermal extruding. After thermal extruding Nd2Fe17B7 magnets, Nd-rich phases are not distributed in the intergranular region on the average and a lot of Nd-rich phases aggregate or separate from the magnet. The results show that the microstructure of Nd-rich is consisted of α-Nd phase and Nd2Fe17 phase, which approaches to eutectic structure of binary Nd-Fe alloy. After adding element Al, Nd2Fe15Al2 phases segregate near to the grain boundary of the magnetic Nd2Fe14B phase, which leads to the improvement of coercivity of magnets.
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