The title complex [Cu3(TFSSB)2·(H2O)4·4H2O]n (TFSSB=taurine 3-formylsalicylic schiff base) was synthesized by TFSSB and copper(Ⅱ) acetate monohydrate in ethanol solution and the crystal structure was determined by X-ray diffraction method. The crystal belongs to monoclinic system, space group P21,with cell parameters: α=0.9279(6)nm, b=1.1730(2)nm, c=1.471(2)nm,β=106.96(2)°, and V=1.531(2)nm3, Z=2, Dc=1.890g·cm-3,μ=2.291mm-1, F(000)=882, R1=0.0259, ωR2=0.0659. The Cul is five-coordinate, the Cu2 is four-coordinate. CCDC: 253298.
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