We capture intermediate of Valsartan analogue's synthesis reaction under hydrothermal condition.The crystal belongs to monoclinic system with space group P21/c, and a=1.089 31(18) nm, b=1.914 6(3) nm, c=0.97273(16) nm, β=104.667(3)°, V=1.962 7(6) nm3, Dc=1.581 g·cm-3, Z=4.CCDC:629930.
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