固体超强酸催化剂SO42-/TiO2-MoO3的制备及其催化合成缩醛(酮)

杨水金; 梁永光; 余协卿; 孙聚堂

首页> 外文期刊>中国化学工程学报（英文版） >固体超强酸催化剂SO42-/TiO2-MoO3的制备及其催化合成缩醛(酮)

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固体超强酸催化剂SO42-/TiO2-MoO3的制备及其催化合成缩醛(酮)

机译：固体超强酸催化剂SO42-/TiO2-MoO3的制备及其催化合成缩醛(酮)

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机译：SO24-/TiO2-MoO3, a novel solid superacid, has been prepared and its catalytic activity at different synthetic conditions was examined with esterification of n-butanoic acid and n-butyl alcohol as probing reaction.The optimum conditions were also found, that is, the mass ratio of MoO3 used in the compound is 25%, the catalytic synthesis of six similar important ketals and acetals as catalyst and revealed high catalytic activity. Under the condition that the molar ratio of aldehyde/ketone to glycol was 1:1.5, the mass ratio of the catalyst to the reactants was 0.5% and the reaction time 1.0 h, the yield of ketals and acetals reached up to 63.2%. The catalyst can be easily recovered and reused.

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来源
《中国化学工程学报（英文版）》 |2005年第1期|51-55|共5页
作者
杨水金; 梁永光; 余协卿; 孙聚堂;
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作者单位

Department of Chemistry and Environmental Engineering Hubei Normal University Huangshi 435002 China;

College of Chemistry and Molecular Sciences Wuhan University Wuhan 430072 China;

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收录信息中国科技论文与引文数据库(CSTPCD);
原文格式 PDF
正文语种 chi
中图分类
关键词
SO42-/TiO2-MoO3; solid superacid; acetalation; katalation;

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专利

1. Selective conversion of cotton cellulose to glucose and 5-hydroxymethyl furfural with SO42/MxOy solid superacid catalyst [J] . Yang, Fang, Li, Yang, Zhang, Qian, Carbohydrate Polymers: Scientific and Technological Aspects of Industrially Important Polysaccharides . 2015,第Null期

机译：SO42 / MxOy固体超强酸催化剂将棉纤维素选择性转化为葡萄糖和5-羟甲基糠醛
2. Fatty acid methyl ester synthesis catalyzed by solid superacid catalyst SO_4~(2-)/ZrO_2-TiO_2/La~(3+) [J] . Yan Li, Xiao-Dong Zhang, Li Sun, Applied Energy . 2010,第1期

机译：固体超强酸催化剂SO_4〜（2-）/ ZrO_2-TiO_2 / La〜（3+）催化合成脂肪酸甲酯
3. A ternary nanooxide NiO-TiO2-ZrO2/SO42- as efficient solid superacid catalysts for electro-oxidation of glucose [J] . Gu Yingying, Yang Haihong, Li Benqiang, Electrochimica Acta . 2016,第Null期

机译：三元纳米氧化物NiO-TiO2-ZrO2 / SO42-作为有效的固体超强酸催化剂，用于葡萄糖的电氧化
4. Preparation of new solid super-acid catalyst, titanium sulfate supported on zirconia and its acid catalytic properties [C] . J.R. Sohn, E-H. Park, J-G. Kim Scientific Bases for the Preparation of Heterogeneous Catalysts . 2002

机译：新型固体超强酸催化剂氧化锆负载硫酸钛的制备及其酸催化性能
5. Synthesis and Characterization of Pt/TiO2/C Composite Catalysts for Fuel Cells Prepared Using a Glucose Modifier. [D] . Odetola, Christopher. 2017

机译：使用葡萄糖改性剂制备的燃料电池Pt / TiO2 / C复合催化剂的合成与表征。
6. Antioxidant and Fluorescence Properties of Hydrogenolyzised Polymeric Proanthocyanidins Prepared Using SO42−/ZrO2 Solid Superacids Catalyst [O] . Liwen Ni, Fanbin Zhao, Bolun Li, Molecules . 2018

机译：SO42- / ZrO2固体超强酸催化剂制备的氢解聚合物原花青素的抗氧化和荧光性质
7. Catalysis of a Nanometre Solid Super Acid of SO42-/TiO2 on the Thermal Decomposition of Ammonium Nitrate [O] . Xiaolan Song, Yi Wang, Dan Song, 2016

机译：纳米固体超强酸sO42- / TiO2催化剂对硝酸铵热分解的催化作用
8. Clean gasoline reforming with superacid catalysts. Quarterly report, July--September 1991. [R] . Davis, B. H. 1993

机译：用超强酸催化剂清洁汽油重整。季度报告，1991年7月至9月。

固体超强酸催化剂SO42-/TiO2-MoO3的制备及其催化合成缩醛(酮)

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