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Performance of Structured Packing in High Pressure Distillation

机译:高压蒸馏中规整填料的性能

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Performance of Mellapak 250Y and 350Y corrugated structured packing in distillation applications at pressures ranging from 0.3 to 2.0MPa is analysed by using HTU-NTU method.These data are obtained in distillation column with 0.15m diameter operated with n-butane/n-pentane system at total reflux.In considering the axial backmixing effects.the height of an overall gas phase transfer unit,HTUOG,is divided into two parts.One part represents the height of an overall gas phase transfer unit,without backmixing, designated as HUTOG,and the other part,designated as the height of a backmixing unit(HBUO),accounts for the backmixing effects.The HTUOG is evaluated from the measured concentration profile of n-butane in liquid phase.The HBUO obtained experimentally is correlated in terms of the properties of the materials being separated and the equivalent diameter of the structured packing.Our result shows that HBUO varies from 0.12 to 0.34m as pressure increases from 1.0 to 1.9MPa.It indicates that the overall efficiency of the structured packing decreas gradually at high pressure,as a result of the vapor backmixing.
机译:使用HTU-NTU方法分析了Mellapak 250Y和350Y波纹结构填料在压力为0.3至2.0MPa的蒸馏应用中的性能,这些数据是在直径为0.15m的蒸馏塔中通过正丁烷/正戊烷系统操作获得的考虑到轴向返混效果,将整个气相转移单元的高度HTUOG分为两部分。一部分代表不进行返混的整个气相转移单元的高度,称为HUTOG,并且另一部分称为回混单元(HBUO)的高度,说明回混效果。HTUOG是根据液相中正丁烷的浓度分布图评估的。通过实验获得的HBUO在性质上相关结果表明,随着压力从1.0到1.9MPa的增加,HBUO在0.12至0.34m范围内变化。由于蒸汽回混,结构化填料的整体效率在高压下逐渐降低。

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