A mild Porco’s two-step, one-pot condensation reaction for the preparation of 3-aryl- 5-phenylselenomethyl 1, 2, 4-oxadiazole through phenylseleno acetic acid and benzamidoxime was reported. And further deselenenylation of 3-aryl-5-phenylselenomethyl 1, 2, 4-oxadiazole was studied.
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