This paper presents a process for preparing high purity tungstentrioxide in which Shizhuyuan high molybdenum scheelite concentrates are treated by molybdenum removal and NaHS extraction of tertiary amine, evaporation and crystallization using the autoclave- soda process. The problems about increasing the recovery ratio of tungsten trioxide and purifying sodium tungstate with additives are also discussed in the paper.%介绍了采用苏打压煮、NaHS除钼、叔胺萃取、蒸发结晶处理柿竹园高钼白钨精矿,生产高纯三氧化钨的工艺。并对加入添加剂以提高三氧化钨回收率、净化钨酸钠溶液等问题进行了探讨。
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