New synthetic condition in a wide temperature range from 110℃ to 190℃ was employed to crystallize DBA-VPI-5. The phase transformation of the samples prepared at different temperatures was measured by high-temperature x-ray diffraction technique.
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机译:Evaluation of structural transformation in 2D metal–organic frameworks based on a 4,4′-sulfonyldibenzoate linker: microwave-assisted solvothermal synthesis, characterization and applications