A novel arsenamolybdate [Ni(dien)2 ]2 [As6 NiMo6 O30 ] ・ 2H2 O (1) (dien = diethyl‐enetriamine) ,has been prepared by hydrothermal methods and structurally characterized by el‐emental analysis ,IR ,TG analysis and single‐crystal X‐ray diffraction analysis .Compound 1 crystallizes in the monoclinic space group P2 (1) .The structure of 1 is constructed from [As6 NiMo6 O30 ]4 - anionic clusters and [Ni(dien)2 ]2 + complex subunits .%利用水热合成法得到了一个结构新颖的砷钼酸盐[Ni(dien)2]2[As6 NiMo6 O30]・2H2 O (1)(dien =二乙烯三胺),并用红外光谱、元素分析、热重分析和 X 射线单晶衍射对之进行了表征。化合物1属于单斜晶系,P2(1)/n 空间群。化合物1是由[As6 NiMo6 O30]4-阴离子簇和[Ni(dien)2]2+配合物构成。
展开▼