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Creep and microstructure in discontinuous metal matrix composites and their matrices.

机译:不连续金属基复合材料及其基体的蠕变和微观结构。

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摘要

High temperature deformation in discontinuous SiC (SiC particulate or SiC whisker) reinforced powder metallurgy 2124 Al composites was investigated for the first time over seven orders of magnitude of strain rate in a temperature range of 618 K-678 K. In order to provide the basis for comparison, the creep behavior of the matrix material--PM 2124 Al alloy was also studied. The experimental results show that the strengthening effect of SiC reinforcement is significant only at low stress range which corresponds to a strain rate lower that 10{dollar}sp{lcub}-5{rcub}{dollar} to 10{dollar}sp{lcub}-4{rcub}{dollar}sec{dollar}sp{lcub}-1{rcub}{dollar}. In high stress range, the strength of SiCp-2124 Al composites is getting close to that of unreinforced 2124 Al alloy. In the stress range used in the present investigation, SiCw-2124 Al is always stronger than 2124 Al alloy, but due to the different curvatures of the stress-strain rate plots for the materials, it can be expected that the strength of SiCw-2124 Al composite could be the same as that of its matrix material--PM 2124 Al alloy at very high stress levels which correspond to a strain rate higher than 10{dollar}sp{lcub}-1{rcub}{dollar}sec{dollar}sp{lcub}-1{rcub}{dollar}. The apparent stress exponent and apparent of activation energy for the materials tested in the present investigation are not constant, rather they are a function of applied stress. It is demonstrated that with an assumption of existence of a threshold stress for creep the abnormal creep behavior of discontinuous SiC-2124 Al composites can be characterized by a modified power law equation. In order to clarify the creep mechanism and the origin of the threshold stress in the materials, transmission electron microscopy (TEM) observations on creep microstructure in 2124 Al specimens were conducted. It is shown that subgrain structures are developed during the deformation and the average size of the subgrains decreases with increasing applied stress. The observation indicates that the rate-controlling process of creep in the materials is high-temperature dislocation climb. This conclusion is consistent with that inferred from the mechanical tests. Other two important features revealed by TEM approaches are (i) the presence of a non-uniform distribution of ultrafine oxide particles (average particle size of 8.8 nm) in the material and (ii) the extensive attractive interaction between the oxide particles and dislocations. This attractive interaction may provide an explanation for the origin of the threshold stress for creep in the materials used in the present investigation.
机译:在618 K-678 K的温度范围内,以七个数量级的应变率首次研究了不连续SiC(SiC颗粒或SiC晶须)增强粉末冶金2124 Al复合材料中的高温变形。为了进行比较,还研究了基体材料PM 2124铝合金的蠕变行为。实验结果表明,仅在低应力范围内,SiC增强的强化作用才显着,这对应于低于10 {dol} sp {lcub} -5 {rcub} {dol}至10 {dol} sp {lcub的应变速率} -4 {rcub} {dollar} sec {dollar} sp {lcub} -1 {rcub} {dollar}。在高应力范围内,SiCp-2124 Al复合材料的强度接近于未增强的2124 Al合金。在本研究使用的应力范围内,SiCw-2124 Al总是比2124 Al合金强,但是由于材料的应力-应变率图的曲率不同,因此可以预期SiCw-2124的强度铝复合材料可以与基体材料-PM 2124铝合金相同,处于非常高的应力水平,对应的应变速率高于10 {dollar} sp {lcub} -1 {rcub} {dollar} sec {dollar } sp {lcub} -1 {rcub} {dollar}。在本研究中测试的材料的表观应力指数和活化能表观不是恒定的,而是施加应力的函数。结果表明,假设存在蠕变的阈值应力,则可以通过修正的幂律方程来表征不连续SiC-2124 Al复合材料的异常蠕变行为。为了阐明材料的蠕变机理和阈值应力的起源,对2124个Al样品的蠕变微观结构进行了透射电子显微镜(TEM)观察。结果表明,在变形过程中形成了亚晶粒结构,并且随着施加应力的增加,亚晶粒的平均尺寸减小。观察表明,材料的蠕变速率控制过程是高温位错爬升。这个结论与从机械测试中得出的结论是一致的。 TEM方法揭示的其他两个重要特征是:(i)材料中存在超细氧化物颗粒(平均粒径为8.8 nm)的不均匀分布,以及(ii)氧化物颗粒与位错之间广泛的吸引力相互作用。这种有吸引力的相互作用可以解释本研究中使用的材料中蠕变的阈值应力的来源。

著录项

  • 作者

    Li, Yong.;

  • 作者单位

    University of California, Irvine.;

  • 授予单位 University of California, Irvine.;
  • 学科 Engineering Mechanical.; Engineering Metallurgy.; Engineering Materials Science.
  • 学位 Ph.D.
  • 年度 1996
  • 页码 184 p.
  • 总页数 184
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

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