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Test development and material characterization of hot poured crack sealant at low temperature.

机译:低温热灌缝密封胶的测试开发和材料表征。

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摘要

Crack sealing has been used extensively as a routine preventative maintenance practice in flexible pavements. It has been shown that if the cracks can be sealed properly, pavement service life can be extended by three to five years. Thus, the most important issue is how to select a proper sealant material in a specific location. Currently, the material selection is based on the American Society for Testing and Materials (ASTM) standards that have been widely reported to correlate poorly with field performance because ASTM specifications do not reflect the viscoelatic nature of sealants. Therefore, it is indeed an urgent need to develop a performance-based guidelines for the selection of hot-poured bituminous crack sealant. In this study, two new test methods were introduced to measure sealant's low temperature rheological properties: the crack sealant bending beam rheometer (CSBBR) test and the crack sealant direct tension tester (CSDTT) test.;The CSBBR test, which is a modification of the bending beam rheometer (BBR) test currently used in the SuperPave(TM) binder specification, was developed to investigate sealant's low temperature flexural property. The major modification to the SuperPave(TM) BBR test was to double the specimen thickness used in the CSBBR test due to the excessive softness of crack sealant compare to bitumen binder. In the CSBBR test, sealant was subjected to a creep loading for 240s following by a 480s of recovery. The three performance parameters calculated from the CSBBR results to evaluate low temperature flexural property of crack sealant were the stiffness at 240s, the average creep rate, and the dissipated energy ratio.;The CSDTT test, which is a modification from the direct tension tester test currently used in the SuperPave(TM) binder specification, was developed to investigate sealant's low temperature tensile property. The test was modified by redesigning its specimen geometry and loading rate to simulate sealant's in-situ condition. The three performance parameters calculated from the CSDTT results to evaluate crack sealant low temperature tensile property were the extendibility, the strain energy density, and the relaxation modulus decay.;Among these six performance parameters, stiffness at 240s of 25MPa, average creep rate of 0.31 mm/mm/s, and extendibility level at different temperatures were identified and proposed as selection criteria for crack sealant at low temperature. These parameters were used to assess several in-service crack sealants with known field performance. The results show that the proposed tests and performance parameters are highly correlated with sealant field performance when compared to current ASTM specification standards.;In addition to the mechanical characterization of the sealant material, microstructure of the sealants were also investigated by confocal laser scanning microscopy (CLSM), environmental scanning electron microscopy (ESEM), gel-permeation chromatography (GPC), Fourier-transform infrared spectroscopy (FTIR), and thermo-gravimetric analysis (TGA). These techniques reveal the composition of sealant as well as the interaction between the components and are used to assist the understanding of various sealant mechanical behaviors. The results of the microstructure analysis show that with polymer modification, the low temperature tensile property of the sealant improves. However, if the ground tire rubber (GTR) is added, the improvement of tensile property is reduced, but the flexural strength is increased.
机译:裂缝密封已被广泛用作柔性路面的常规预防性维护措施。已经表明,如果裂缝能够被正确地密封,则路面使用寿命可以延长三到五年。因此,最重要的问题是如何在特定位置选择合适的密封材料。当前,材料的选择基于美国材料试验协会(ASTM)的标准,该标准已被广泛报道与现场性能之间的相关性很差,因为ASTM规范并未反映密封胶的粘胶特性。因此,确实迫切需要开发一种基于性能的指南,以选择热浇注的沥青裂缝密封剂。在这项研究中,引入了两种新的测试方法来测量密封剂的低温流变性能:裂缝密封剂弯曲梁流变仪(CSBBR)测试和裂缝密封剂直接张力测试仪(CSDTT)测试.CSBBR测试是对密封剂的改进。为了研究密封胶的低温弯曲性能,开发了目前在SuperPave™粘合剂规格中使用的弯曲束流变仪(BBR)测试。 SuperPave TM BBR试验的主要改进是将CSBBR试验中使用的样品厚度加倍,因为与沥青粘合剂相比,裂缝密封剂的柔软度过高。在CSBBR测试中,密封剂承受了240 s的蠕变载荷,随后恢复了480 s。根据CSBBR结果计算出的三个性能参数,用于评估裂缝密封胶的低温挠曲性能,其在240s时的刚度,平均蠕变速率和耗散能量比。CSDTT试验是对直接拉伸试验机试验的改进目前用于SuperPave(TM)粘合剂规范中的粘合剂是为了研究密封胶的低温拉伸性能而开发的。通过重新设计试样的几何形状和加载速率以模拟密封胶的原位条件,对试验进行了修改。根据CSDTT结果计算出的三个性能参数,分别是可扩展性,应变能密度和松弛模量衰减,以评估裂缝密封胶的低温拉伸性能。其中六个性能参数在240s时的刚度为25MPa,平均蠕变率为0.31。确定了mm / mm / s以及在不同温度下的可扩展性水平,并提出了低温裂缝密封胶的选择标准。这些参数用于评估几种已知现场性能的在役裂缝密封胶。结果表明,与当前的ASTM规范标准相比,所提出的测试和性能参数与密封剂的现场性能高度相关。;除了对密封剂材料进行机械表征外,还通过共聚焦激光扫描显微镜研究了密封剂的微观结构( CLSM),环境扫描电子显微镜(ESEM),凝胶渗透色谱(GPC),傅立叶变换红外光谱(FTIR)和热重分析(TGA)。这些技术揭示了密封胶的成分以及各组分之间的相互作用,并用于帮助理解各种密封胶的机械性能。微观结构分析结果表明,通过聚合物改性,提高了密封胶的低温拉伸性能。但是,如果添加了地面轮胎橡胶(GTR),则抗拉性能的改善会降低,但抗弯强度会提高。

著录项

  • 作者

    Yang, Shih-Hsien.;

  • 作者单位

    University of Illinois at Urbana-Champaign.;

  • 授予单位 University of Illinois at Urbana-Champaign.;
  • 学科 Engineering Civil.
  • 学位 Ph.D.
  • 年度 2009
  • 页码 205 p.
  • 总页数 205
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 建筑科学;
  • 关键词

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