It has previously been predicted that materials that have a simultaneous negative permittivity and negative permeability, called left-handed materials (LHM), will possess very unusual properties, such as negative refraction, inverse Doppler effect, and reversed Cherenkov radiation. In this dissertation I present results from microwave experiments designed to confirm that LHMs will exhibit negative refraction. I also present a discussion about the LHM design, and numerical, electromagnetic simulations. The experiments presented here include transmission experiments, refraction experiments, and surface plasmon experiments. The refraction experiments in Chapter 4 directly observe negative refraction for the first time. The results from the other experiments are consistent with theoretical models and support the claim that negative refraction has been observed.; The materials used in the experiments presented here are fabricated, structured materials that contain fiberglass and copper with unit cell parameters on the order of millimeters. Metamaterials have been defined as being composite materials whose bulk properties are different than those of the constituent materials. By this definition, the LHMs used here are metamaterials, so long as the wavelength of the electromagnetic waves being used to probe the LHM are longer than the unit cell parameter.
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