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A Study of the Effects of Laser Shock Peening on Residual Stress, Microstructure and Local Properties of IN718 Nickel-Base Superalloy.

机译:激光冲击喷丸对IN718镍基高温合金的残余应力,微观结构和局部性能的影响研究。

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摘要

In this project effects of Laser shock peening (LSP) on two aero engine alloys, IN718 and IN718 SPF were studied. The primary goal of the program was to secure required fundamental knowledge of e impact of LSP process parameters on these two aero engine alloys and thereby advance the science and application base of this process to other materials and parts. The research program designed accordingly includes the following key elements: 1) Developing LSP process parameters for typical Ni base aero engine alloys; (2) characterization of surface and sub-surface macro and micro residual strains/stresses a function of LSP process parameters (3) characterization of microstructural changes as a function of LSP process parameters and; (4) Study Thermal relaxation of residual stresses and understand the underlying kinetics.;Firstly, different LSP process parameters including: Power density, impact overlaps, ablative overlays and coverage were studied to impart deep compressive residual stresses to the near surface regions of peened coupons. A host of different techniques were then used to characterize distribution of residual stresses/strains, roughness, hardness, plastic strains and microstructure. Role of ablative layer was also investigated. Samples were peened using an ablative layer different ablative layers (black vinyl tape, aluminum tape) and without an ablative layer and compared in terms of topography, residual stress fields and microstructure.;Two different diffraction based techniques were used to characterize residual stress fields: conventional X-ray diffraction and Synchrotron X-ray diffraction (SXRD). Conventional X-ray coupled with electro polishing offers a fast means of analyzing residual stresses, while SXRD enables high resolution, non-destructive characterization of strains/stresses. Experiments showed that higher power density lead to compressive residual stresses which were higher in magnitude in near surface regions. There is a saturation power density, after which any increase in power density did not result in further increase in magnitude and depth residual stresses.;Plastic deformation introduced by LSP was characterized using a variety of tools including hardness measurements (micro hardness with a knoop's indenter and nano indentation), analyzing full width half maximum of diffraction peaks, micro pillar compression tests and electron back scattered diffraction. Results indicated that LSP does not introduce high plastic strain in the material. This was evident in moderate increase in hardness (∼20%), a small increase in FWHM of diffraction peaks and a small increase in low angle misorientations (obtained using EBSD). Using all these techniques it was determined that the plastic deformation introduced by peening extended 300–500 µm from the peened surface.;Microstructure of as-received and peened samples was studied using optical microscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Electron back scattered Diffraction (EBSD). Peened samples showed no grain refinement (unlike conventional shot peening) or change in chemistry. TEM revealed increase in dislocation density in near surface regions, which decreased as a function of distance.;Thermal relaxation of both macro and micro residual strains/stresses and microstructure stability at selected temperatures as a function of time will be studied using the same tools and the kinetics of relaxation modeled from the data obtained.
机译:在该项目中,研究了激光冲击喷丸(LSP)对两种航空发动机合金IN718和IN718 SPF的影响。该计划的主要目标是确保获得有关LSP工艺参数对这两种航空发动机合金的影响的基本知识,从而将该工艺的科学和应用基础推进到其他材料和零件。据此设计的研究计划包括以下关键要素:1)为典型的镍基航空发动机合金开发LSP工艺参数; (2)表征表面和亚表面宏观和微观残余应变/应力与LSP工艺参数的关系;(3)表征微观结构变化与LSP工艺参数的关系;以及(4)研究残余应力的热松弛并了解其基本动力学。首先,研究了不同的LSP工艺参数,包括:功率密度,冲击重叠,烧蚀覆盖层和覆盖率,以对锤击试样的近表面区域施加深压缩残余应力。 。然后使用许多不同的技术来表征残余应力/应变,粗糙度,硬度,塑性应变和微观结构的分布。还研究了烧蚀层的作用。使用不同的烧蚀层(黑色乙烯基胶带,铝胶带)和不使用烧蚀层的烧蚀层对样品进行喷丸处理,并在形貌,残余应力场和微观结构方面进行比较;使用两种基于衍射的不同技术表征残余应力场:常规X射线衍射和同步加速器X射线衍射(SXRD)。传统的X射线与电抛光相结合提供了一种分析残余应力的快速方法,而SXRD可以实现高分辨率的应变/应力的非破坏性表征。实验表明,较高的功率密度会导致压缩残余应力,该残余应力在表面区域附近的强度较高。有一个饱和功率密度,此后功率密度的任何增加都不会导致强度和深度残余应力的进一步增加。LSP引入的塑性变形使用多种工具进行了表征,包括硬度测量(带有努氏压头的微硬度)和纳米压痕),分析衍射峰的全宽一半最大值,微柱压缩测试和电子反向散射衍射。结果表明,LSP不会在材料中引入高塑性应变。这在硬度适度增加(约20%),衍射峰的FWHM略有增加以及低角度取向不良(使用EBSD获得)方面略有增加是明显的。使用所有这些技术,可以确定通过喷丸处理从喷丸表面延伸出300-500 µm所引起的塑性变形。;使用光学显微镜,扫描电子显微镜(SEM),透射电子显微镜研究了接收和喷丸样品的微观结构( TEM)和电子背散射衍射(EBSD)。喷丸后的样品未出现晶粒细化(与常规喷丸不同)或化学变化。透射电镜(TEM)揭示了近表面区域中位错密度的增加,随距离的增加而减小。;将使用相同的工具研究在选定温度下宏观和微观残余应变/应力的热弛豫以及随时间变化的微观结构稳定性。根据获得的数据模拟松弛动力学。

著录项

  • 作者

    Gill, Amrinder Singh.;

  • 作者单位

    University of Cincinnati.;

  • 授予单位 University of Cincinnati.;
  • 学科 Engineering Materials Science.
  • 学位 Ph.D.
  • 年度 2012
  • 页码 341 p.
  • 总页数 341
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

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