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Using multi-layered roll bonding and reaction annealing to process gamma-titanium aluminide sheet material.

机译:使用多层辊压结合和反应退火来处理γ-钛铝化物片材。

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摘要

The process of roll bonding and reaction annealing was used to process gamma-titanium aluminide sheets with a nearly fully lamellar microstructure. Cold roll bonding was employed to bond elemental Al and Ti foils. The bonded sheets were annealed at 600 °C to convert all of the Al into TiAl3. The effect of rolling strain on the reaction kinetics was studied. Accumulative roll bonding was also employed to study the effect of increased rolling strain on the microstructures resulting after annealing. After the first annealing stage, a cold rolling step resulted in a denser microstructure. A second annealing treatment at 1300 °C for 6 h resulted in a microstructure consisting of two phases, gamma and alpha2, along with Kirkendall porosity. Further densification of the sheets was carried out using hot rolling. A final heat treatment at 1400 °C for 0.3 h resulted in nearly fully lamellar microstructure. The porosity evolution was evaluated at different stages of processing. The mechanical properties of the processed sheet were determined and compared with the data available in the literature.; The process of bi-metal multi-layer roll bonding was modeled using the equilibrium force balance method (slab method). The effect of anisotropy and strain hardening was included in the model. The effect of different variables such as total reduction, coefficient of friction, roll radius and initial foil thickness ratio, on the thickness fraction of metals in the bonded composite was investigated. The model enables the estimation of the final composition of the roll bonded composite. The results of the model were compared with the experimental results, and good agreement was observed.
机译:辊压结合和反应退火的过程被用于处理具有几乎完全层状微结构的γ-钛铝化物片。采用冷轧粘结来粘结元素铝箔和钛箔。将粘合的片材在600°C下退火,以将所有的Al转化为TiAl3。研究了轧制应变对反应动力学的影响。累积轧制粘结也被用来研究轧制应变增加对退火后产生的微观结构的影响。在第一退火阶段之后,冷轧步骤导致致密的微观结构。在1300°C下进行了6h的第二次退火处理,形成了由两个相gamma和alpha2以及Kirkendall孔隙率组成的微观结构。片材的进一步致密化使用热轧进行。在1400°C下进行的最终热处理0.3 h导致了几乎完全的层状微结构。在加工的不同阶段评估了孔隙度的演变。确定了加工过的板材的机械性能,并与文献中的数据进行了比较。使用平衡力平衡法(平板法)对双金属多层辊压粘合过程进行建模。该模型包括各向异性和应变硬化的影响。研究了不同的变量,如总压下率,摩擦系数,辊半径和初始箔厚度比,对粘结复合材料中金属的厚度分数的影响。该模型能够估计辊压复合材料的最终成分。将模型的结果与实验结果进行比较,观察到良好的一致性。

著录项

  • 作者单位

    The University of Alabama.;

  • 授予单位 The University of Alabama.;
  • 学科 Engineering Metallurgy.; Engineering Materials Science.
  • 学位 Ph.D.
  • 年度 2005
  • 页码 134 p.
  • 总页数 134
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 冶金工业;工程材料学;
  • 关键词

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