光固化三维多孔丙烯酸酯膜(二氧化硅--碳(SiO2--C))和季铵盐氟预聚物的抗菌和电化学应用

目录

声明

ACKNOWLEDGEMENTS

ABSTRACT

摘要

Table of contents

Chapter 1 Introduction and Literature Review

1．1 Historical Background

1．2 General Membrane classification with their Applications

1．3 General synthesis methods for porous membrane

1．4 SiO2-C Membrane synthesis procedures and its Applications

1．4．1 Designed structures

1．5 Objectives of this work

1．6 Novelty statement

1．2 Binary phase solid state Photo-Polymerization behavior of porous acrylate membrane using different irradiation sources

1．2．1 Introduction

1．3 Synthesis of Quaternized fluorine-containing polyacrylic acrylate (QFPAA) for antimicrobial Application

1．3．1．Introduction

1．3．2 PROBLEM STATEMENT

Chapter 2 Materials and Methods

2．1．2 Synthesis of Photo cured 3D-porous membrane (SiO2-C material)

2．1．3 Electrochemical measurements

2．1．4 Material Characterization

2．2．1 Materials

2．2．2 Fabrication of Porous membrane (Cryogels)

2．2．3 Characterization

2．3 Synthesis of Quaternized fluorine-containing polyacrylic acrylate (QFPAA) for antibacterial Application

2．3．1 Synthesis of 18 quaternary ammonium salt

2．3．2 Synthesis of Quaternized Fluorine polyacrylic acrylate

2．3．3 Preparation of UV curing system

2．3．4 Characterization

Chapter 3 Results and Discussions

3．1．2 Brunauer-Emmett-Teller (BET)，X-ray photoelectron spectroscopy (XPS) Analysis and Raman spectrum analysis

3．1．3 Microstructure Characterization

3．1．4 Electrochemical performances

3．2 Binary phase solid state Photo-Polymerization performance of acrylate membrane (cryogels) using different irradiation sources

3．2．1 Photo DSC

3．2．2 FT-IR analysis

3．2．3 Morphological study

3．2．4 UV-vis analysis

3．2．5 Water intake ratio and Percentage of porosity (P％)

3．2．6 Thermal stability

3．2．7 Biodegradation degree

3．3 Synthesis of Quaternized fluorine-containing polyacrylic acrylate (QFPAA) for antimicrobial Application

3．3．1 Fourier transform infrared spectroscopy spectra of Quaternary ammonium salt

3．3．2 1HNMR of Quaternary ammonium salt

3．3．3 X-ray photoelectron spectroscopy (XPS)

3．3 Fourier transform infrared spectroscopy spectra of quaternized fluorine containing prepolymer

Chapter 4 Conclusion

5．Publications

References