首页> 外文会议>The Waterborne Symposium "Advances in Sustainable Coatings Technology" >ACCELERATING COATING RD BY AUTOMATED HIGH OUTPUT TECHNOLOGIES
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ACCELERATING COATING RD BY AUTOMATED HIGH OUTPUT TECHNOLOGIES

机译:自动化的高产量技术加速涂层研发

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The development and design of new polymeric materials are based on the synthesis of new compounds and the optimization of existing materials. Therefore, researchers have to synthesize a large amount of (co)polymers and screen many reaction conditions by varying, e.g., monomers, catalysts, molecular weights, reaction times, reaction temperatures, feed rates, etc. This is a very time-consuming process. In order to speed up this research, parallel experimentation and high-output methods represent a very promising approach: Many different parameters can be investigated simultaneously or in fast serial mode and the results easily can be compared. This eventually will result in new structure property relationships. Therefore, Polymer science is a field that provides a seemingly inexhaustible playground for polymer chemists due to the vast experimental parameter space. Using selected examples, from the Polymer and Coating Industry, this presentation will show how a variety of very challenging workflows fully have been automated using a parallel set-up of individually controlled batch reactors. Parameters like feed rates, temperature, pH, agitation, pressure and viscosity actively can be controlled for each of the reactors, which allows researchers to characterize und understand even complex chemical processes in great detail while allocating only limited resources (in terms of time and researchers) at the same time. As a consequence a significant productivity increase per FTE (Full Time Equivalent) might be achieved.
机译:新聚合物材料的开发和设计基于新化合物的合成和现有材料的优化。因此,研究人员必须合成大量的(共)聚合物,并通过改变例如单体,催化剂,分子量,反应时间,反应温度,进料速率等来筛选许多反应条件。这是一个非常耗时的过程。为了加快这项研究,并行实验和高输出方法代表了一种很有前途的方法:可以同时或以快速串行模式研究许多不同的参数,并且可以轻松地比较结果。这最终将导致新的结构属性关系。因此,由于广阔的实验参数空间,高分子科学领域为高分子化学家提供了看似无法取胜的场所。使用来自聚合物和涂料行业的精选示例,本演示将展示如何使用并行控制的独立控制的间歇式反应器将各种非常具有挑战性的工作流程完全自动化。可以动态控制每个反应器的进料速率,温度,pH,搅拌,压力和粘度等参数,这使研究人员能够表征和理解甚至非常复杂的化学过程,同时仅分配有限的资源(在时间和研究人员方面) ) 与此同时。结果,可以实现每FTE(全时等效)的显着生产率提高。

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