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Dislocation Dynamics in Intermetallic and Oxide Dispersion Strengthened (ODS) Alloys

机译:金属间和氧化物弥散强化(ODS)合金中的位错动力学

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In situ straining experiments in a high-voltage electron microscope allow the observation of the dynamic behaviour of individual dislocations. Such experiments have been performed on the intermetallic alloys NiAl, NiAl containing 0.2 at% Ta, γ-TiAl, and MoSi_2, and the oxide dispersion strengthened (ODS) alloys INCOLOY MA956 and INCONEL MA754 in a wide range of temperatures. There are many similarities in the dynamic behaviour of dislocations in the different materials. In the intermetallic alloys, a transition occurs between low temperature mechanisms and a viscous motion in the temperature range of the flow stress anomaly. The viscous motion at high temperatures can be explained by diffusion processes in the dislocation cores, which can be described by the theory of the Cottrell effect. The diffusing species can be quite different, alloying components or intrinsic point defects like vacancies and antisite defects existing in the lattice or only in the dislocation cores. If the dislocations are straight and crystallographically oriented during their motion, they may be dissociated and move by a succession of glide and conservative climb between the partial dislocations, to the ODS alloys, the dislocations move between the oxide particles again in a viscous way. The relation between the dislocation dynamics and the strain rate sensitivity of the flow stress is discussed for the different materials.
机译:高压电子显微镜中的原位应变实验可以观察单个位错的动力学行为。已经在宽温度范围内对金属间合金NiAl,含0.2at%Ta的NiAl,γ-TiAl和MoSi_2以及氧化物弥散强化(ODS)合金INCOLOY MA956和INCONEL MA754进行了此类实验。不同材料中位错的动力学行为有很多相似之处。在金属间合金中,在流动应力异常的温度范围内,在低温机理与粘性运动之间发生过渡。高温下的粘性运动可以通过位错核中的扩散过程来解释,这可以通过Cottrell效应理论来描述。扩散物质可能完全不同,合金成分或内在点缺陷(例如,晶格中或仅在位错核中存在的空位和反位缺陷)。如果位错在运动过程中是直的且在晶体学上取向的,则它们可以通过部分位错之间的一连串滑移和保守爬升而离解并移动到ODS合金,位错再次以粘性方式在氧化物颗粒之间移动。讨论了不同材料的位错动力学与流变应力应变率敏感性之间的关系。

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