首页> 外文会议>Seeheim Conference on Magnetism(SCM2004); 20040627-0701; Seeheim(DE) >Iron/graphite core-shell structured nanoparticles prepared by annealing of Fe-C-N composite
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Iron/graphite core-shell structured nanoparticles prepared by annealing of Fe-C-N composite

机译:Fe-C-N复合材料退火制备的铁/石墨核-壳结构纳米粒子

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We are reporting the core-shell structured iron/graphite nanoparticles formed during annealing of the nanopowder prepared by laser pyrolysis of gas phase reactants. The originally synthesized Fe-C-N based nanocomposite powder has been characterized by TEM, XRD and magnetic measurements. Nanopowder was heated up to 800℃ at ~ 1 Pa vacuum. Presence of iron nanoparticles with the mean diameter of 40 nm in the annealed state of nanopowder was proved by XRD and TEM. Moessbauer spectroscopy was used for characterization of the synthesized/annealed nanopowder.
机译:我们报道了通过气相反应物的激光热解制备的纳米粉末的退火过程中形成的核-壳结构的铁/石墨纳米颗粒。最初合成的Fe-C-N基纳米复合粉末已经通过TEM,XRD和磁测量进行了表征。将纳米粉末在〜1 Pa的真空下加热到800℃。 XRD和TEM证实了纳米粉末在退火状态下平均直径为40 nm的铁纳米颗粒的存在。 Moessbauer光谱用于表征合成/退火的纳米粉。

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