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Microstructure and Properties of Pure Zirconium After Irradiation by Charged Particles

机译:带电粒子辐照后纯锆的显微组织和性能

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In order to estimate the possible application of zirconium-based alloy in space craft, the space irradiation effects have been studied using ground simulation testing of a model material, pure zirconium, in this paper. The irradiation tests of charged particles such as protons, argon ion and nitrogen ion on a pure zirconium, UNS R60702 (denoted as Zr 702 herewith), was carried out in a ground space simulation irradiation facility.X-ray diffractometry (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), Nanoindentation, dynamic mechanical analyzis (DMA) and tensile testing were employed to examine the microstructure and properties of the proton, nitrogen ion or argon ion irradiated Zr 702.It is shown that after irradiation with 120 keV protons and argon or nitrogen ions, the specimen surface morphology practically did not change and no new phases could be detected within the surface layer of Zr 702. Dislocation configurations in the irradiated region of Zr 702 were however affected by proton and nitrogen and argon ion irradiation. The bulk mechanical properties such as tensile strength and fracture strain of Zr 702 were mostly not influenced by 120 keV protons and argon or nitrogen ion irradiation. The local properties such as nano-hardness of the irradiated surface were found to vary with the fluence or type of the charged particles.
机译:为了估算锆基合金在航天器中的可能应用,本文使用模型材料纯锆的地面模拟测试研究了空间辐照效果。在地面模拟辐射设备中对纯锆(UNS R60702,以下称为Zr 702)上的质子,质子,氩离子和氮离子等带电粒子进行辐照试验.X射线衍射(XRD),透射用电子显微镜(TEM),扫描电子显微镜(SEM),纳米压痕,动态力学分析(DMA)和拉伸试验来检验质子,氮离子或氩离子辐照Zr 702的微观结构和性能。用120 keV质子和氩或氮离子辐照,样品表面形态实际上没有变化,在Zr 702的表层内未检测到新相。但是,Zr 702辐照区域的位错构型受到质子和氮的影响和氩离子辐照。 Zr 702的整体机械性能(如拉伸强度和断裂应变)大部分不受120 keV质子和氩气或氮离子辐射的影响。发现局部性质例如被辐照表面的纳米硬度随带电粒子的注量或类型而变化。

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