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Investigation of Static Recrystallization Behavior of 9Ni Steels during Thermomechanical Processing

机译:9Ni钢热机械加工过程中静态再结晶行为的研究。

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In order to study the workability and optimise the hot deformation processing parameters for 9Ni steels, the static recrystallization behavior in austenite region was investigated by isothermal double-hit compression on a Gleeble 3800 thermo-simulator. In this paper,two offset methods(2% offset method and 0. 2% offset method) were employed to measure the softening rate. The results showed that the soitemng rate measured by 0. 2% onset method commonly used by other authors was higher than by the 2% offset method, especially the inter-pass time was less than 60 s. The softening fration increased with increasing strain rate,strain of the first pass ,and decreasing the initial grain sise indicated that higher strain energy and less time for recovery had produced higher nucleation rate for the recrystalliaation of 9Ni steels. Relationships between initial grain size, strain in the first pass deformation, stain rate, and, the time for 50% re crystallization, t0.5 , were established by liner regressions. The active energy for static re crystallization was determined to be 194 kj/mol based on the values measured by using the 2% onset method. Ihe equation lor static recrystallization kinetics was established, in which the Avrami exponent was temperature dependant as n,=0. 0023 exp(6948/T) , and had great difference from those of plain carbon steels. Recrystallization fractions deformed at 900T: with different inter-pass times were measured by using the optical microscope and compared with predicted results. The calculated results based on the 2% offset method were in better agreement with the measured values than the 0.2% offset method, indicated that the 2% offset method could better exclude recovery effects when plastric deformation occurred.
机译:为了研究9Ni钢的可加工性并优化其热变形工艺参数,在Gleeble 3800热模拟仪上通过等温双冲击压缩研究了奥氏体区域的静态再结晶行为。本文采用两种补偿方法(2%补偿法和0. 2%补偿法)测量软化率。结果表明,其他作者常用的0. 2%起始法测得的测速率高于2%偏移法测得的测速速率,尤其是通过时间小于60 s。软化率随应变率的增加,初次通过的应变的增加以及初始晶粒尺寸的减小而增加,这表明较高的应变能和较少的恢复时间为9Ni钢的重结晶产生了较高的成核率。通过线性回归建立了初始晶粒尺寸,首过变形中的应变,着色率以及50%再结晶时间t0.5之间的关系。基于通过使用2%开始法测量的值,将静态再结晶的活性能量确定为194kj / mol。建立了静态再结晶动力学方程,其中Avrami指数与温度相关,n = 0。 0023 exp(6948 / T),与普通碳素钢有很大的不同。通过使用光学显微镜测量900T时变形的重结晶分数:具有不同的通过时间,并将其与预测结果进行比较。基于2%偏移量法的计算结果与0.2%偏移量法的测量值更加吻合,表明2%偏移量法可以更好地排除塑性变形发生时的恢复效果。

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