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A novel synthesis of Co Au nanoparticles and characterization

机译:Co Au纳米粒子的新型合成及其表征

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摘要

A homogeneous non-aqueous solution reactions method has been developed to prepare gold-coated cobalt (Co@Au) nanoparticles. After the samp le was washed with 8% HCl, XRD (X-Ray Diffraction), TEM (transmission electron microscopy), and magnetic measurements SQUID (Superconducting Quantum Interference Device) are utilized to characterize the nanocomposites. XRD shows the pattern of sample, which is only responding to gold. TEM results show that the average size of Co@Au nanoparticles is about 10 nm and we can find core-shell structure of the sample. SQUID results show that the particles are ferromagnetic materials at 300K. So the gold-coated cobalt nanoparticles (Co@Au) can be successfully prepared by the homogeneous non-aqueous approach. This kind of core-shell materials is stable in acid condition, which would give many opportunities for bio- application.
机译:已经开发出一种均相的非水溶液反应方法来制备金包被的钴(Co @ Au)纳米颗粒。用8%HCl洗涤样品后,利用XRD(X射线衍射),TEM(透射电子显微镜)和磁测量SQUID(超导量子干涉仪)表征纳米复合材料。 XRD显示样品的图案,该图案仅响应金。 TEM结果表明,Co @ Au纳米粒子的平均粒径约为10 nm,可以发现样品的核-壳结构。 SQUID结果表明,该颗粒是300K的铁磁材料。因此,可以通过均相非水法成功制备金包覆的钴纳米颗粒(Co @ Au)。这种核壳材料在酸性条件下是稳定的,这将为生物应用提供许多机会。

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