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Fabrication of Al-based FGM Containing TiO_2 Nano-Particles by a Centrifugal Mixed-Powder Method

机译:离心混合粉末法制备含TiO_2纳米颗粒的铝基FGM

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Centrifugal method is often applied as the fabrication process of Functionally Graded Materials (FGMs). This is because that this processing method can fabricate FGMs with large size, easily. However, this processing method has a serious problem, namely it is difficult to disperse particles with small size and low wet ability with matrix. Many of powders with nano or very fine particle size often have attractive attention as functional materials. Therefore the above problem of the centrifugal method should be improved. In this study, we proposed a centrifugal mixed-powder method as novel processing technique for the fabrication of FGM containing nano-particle. On first of this processing, powder mixture of functional nano-particle and matrix material is inserted into rotating mold. After that, matrix ingot is melted in crucible and then the molten matrix is poured into the rotating mold with powder mixture, and then, powder of matrix material will be melted by the heat from molten matrix poured from crucible. Finally, an FGM ring with functional nano-particles distributed on its surface can be obtained. Using this processing method, Al-based FGM containing TiO_2 nano-particles on its surface could be fabricated. TiO_2 particle has approximately 500nm in diameter. From microstructural observation, it was found that TiO_2 particles were successfully distributed on surface of FGM ring. Also, hardness on the surface of the FGM ring was higher than that on inner part due to the dispersion hardening.
机译:离心方法通常用作功能梯度材料(FGM)的制造过程。这是因为该处理方法可以容易地制造大尺寸的FGM。但是,该处理方法存在严重的问题,即难以将小粒径且湿润能力低的粒子分散在基质中。许多具有纳米或非常细的粒度的粉末通常作为功能材料引起人们的注意。因此,应该改善离心方法的上述问题。在这项研究中,我们提出了一种离心混合粉末法作为制造含FGM纳米颗粒的新工艺。首先,将功能性纳米颗粒和基质材料的粉末混合物插入旋转模具中。之后,将基体锭料在坩埚中熔化,然后将熔融基体与粉末混合物倒入旋转模具中,然后,从坩埚倒出的熔融基体中的热量将基体材料粉末熔化。最后,可以获得在其表面上分布有功能纳米颗粒的FGM环。使用这种加工方法,可以制造在其表面上含有TiO_2纳米粒子的Al基FGM。 TiO_2颗粒的直径约为500nm。从微观结构观察发现,TiO_2颗粒成功地分布在FGM环的表面。另外,由于分散硬化,FGM环的表面的硬度高于内部的硬度。

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