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Synthesis and Characterization of Boron Nitride Nanotubes-Polycaprolactone Nanocomposite

机译:氮化硼纳米管-聚己内酯纳米复合材料的合成与表征

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This work aimed to investigate the effects of boron nitride nanotubes (BNNTs) on the mechanical and thermal properties of BNNT-polycaprolactone (PCL) nanocomposites. BNNTs were synthesized via co-precipitation and annealing process by using amorphous boron powder as a precursor. PCL-BNNT nanocomposites were prepared by using sonication and thermal curing. Their morphology, thermal and tensile properties were characterized. Morphological observation revealed that BNNTs were arbitrarily and evenly dispersed within the PCL which indicated a good dispersion of the nanotubes in polymer matrix. Both the thermal stability and mechanical properties of neat PCL were enhanced with the addition of BNNTs to polymer matrix, in particular the tensile strength of PLC was increased by 101% with the addition of 5 wt% nanofillers.
机译:本工作旨在研究氮化硼纳米管(BNNT)对BNNT聚己内酯(PCL)纳米复合材料力学和热性能的影响。以非晶态硼粉为前驱体,通过共沉淀和退火工艺合成了BNNTs。采用超声和热固化法制备了PCL-BNNT纳米复合材料。对其形貌、热性能和拉伸性能进行了表征。形态学观察显示,BNNTs在PCL中任意且均匀地分散,这表明纳米管在聚合物基体中具有良好的分散性。在聚合物基体中添加BNNTs后,纯PCL的热稳定性和力学性能都得到了提高,尤其是添加5 wt%纳米填料后,纯PCL的拉伸强度提高了101%。

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