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VISUALISATION AND ANALYSIS OF LDPE MELT FLOWS IN A COEXTRUSION GEOMETRY

机译:LDPE熔体在共挤出几何中的可视化和分析

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Two low density polyethylene melts are studied using a coextrusion flow visualisation cell. The cell design enabled two melt streams to be observed at the confluent region and into the die land to the die exit. The melt streams converge at an angle of 30° and flow into a common die land of 1.0 mm height. The relative stream velocities, hence layer thickness ratio, of the two streams was varied using a restriction plate in one of the streams. Stress and velocity fields are quantified using stress birefringence and particle image velocimetry techniques. Numerical simulation is conducted using flow history dependent viscoelastic stress calculation based on a modified Leonov model and Flow 2000? software. Simulated stress fields are compared to those experimentally. The simulated stress magnitudes were in good agreement with those determined experimentally. The simulation predicted a high local extensional stress in the minor flow stream just upstream of the entry to the die land. This local stress was also observed in the stress birefringence pattern. Extrudate instability was noted even when the stress field (birefringent pattern) in the convergent region and the beginning of the die land was stable. However, disturbances were noted in the birefringence and velocity fields near the exit of the die land when the major stream - minor stream layer thickness ratio was greater than 1.5:1. Surface distortion appeared on the surface of the extrudate on the side of the minor flow stream when process conditions promoted instability. The recently proposed TNSD sign criterion has been used to predict the onset of the wave interfacial instabilities in the coextrusion geometry and good agreement with the experimental observation has been found.
机译:使用共挤出流动可视化细胞研究了两个低密度聚乙烯熔体。电池设计使得在汇合区域中能够观察到两个熔体流,并进入模具到模具出口。熔体流以30°的角度聚集并流入1.0mm高度的常见模具。在其中一个流中的限制板中,两个流的相对流速度因此层厚度比。使用应力双折射和粒子图像速度技术量化应力和速度场。使用基于修改的Leonov模型和流动2000的流动历史依赖性粘弹性应力计算进行数值模拟?软件。模拟应力场与实验相比。模拟应力大小与实验确定的那些吻合良好。该模拟预测了在进入芯片的进入的上游的次要流动流中的高局部延伸应力。在应力双折射模式中也观察到这种局部应力。即使收敛区域和模具开头稳定的应力场(双折射图案)稳定,也注意到挤出物不稳定性。然而,当主要流次微小流层厚度大于1.5:1时,在模具陆出出口附近的双折射和速度场中,在双折射和速度场中注意到干扰。当工艺条件促进不稳定性时,在少量流动流侧的挤出物表面上出现表面畸变。最近提出的TNSD符号标准已用于预测共挤出几何形状中的波浪界面不稳定性的发作,并发现了与实验观察的良好一致性。

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