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Field Applications of Ion Mobility Spectrometry

机译:离子迁移光谱法的现场应用

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摘要

Ion mobility spectrometry (IMS) is an excellent tool for detection of controlled substances under field conditions. Plasmagrams and tables showing the results of field applications will be discussed. Residues of drugs, such as cocaine and heroin, can be left anywhere including vehicles, boats, and houses. In houses, the carpets, walls, and floors are good locations for residues to adhere. Individual clothing can also be contaminated with drug residue. Vehicles that are suspected of having previously smuggled illegal substances can b e vacuumed and screened. Tablets that look similar and respond the same when screened with the Marquis reagent can be differentiated by IMS. With Southern California being the "methamphetamine capital of the world" and the resurgence of phencyclindine (PCP), IMS has proven extremely valuable in the screening of abandoned clandestigne alboratory sites and vehicles in which the clandestine laboratories' chemicals and glassware were transported. IMS is very responsive to ephedrine/pseudoephedrine, a precursor of methamphetamine and 1-piperidinocyclohexanecarbonitrile (PCC), an intermediate of phencylindine. Once residues are detected, vacuumsamples, and/or metanol wipes are collected and analyzed at the DEA Laboratory for confirmaton of the suspected substance using GC-IRD or Mass Spectrometry.
机译:离子迁移光谱(IMS)是用于在现场条件下检测受控物质的优异工具。将讨论显示现场应用结果的表格和表。药物的残留物,如可卡因和海洛因,可以留下包括车辆,船只和房屋的任何地方。在房屋中,地毯,墙壁和地板是残留物粘附的好地方。单个衣服也可以污染药物残留物。怀疑以前走私的非法物质的车辆可以吸尘和筛选。当用侯爵试剂筛选时,看起来相似和响应的平板电脑可以通过IMS来差异化。随着加利福尼亚州的“世界甲基苯丙胺基本”和腓尼汀(PCP)的复苏,IMS在筛查废弃的秘密肉玻璃场和车辆被运输的车辆中被证明是非常有价值的。 IMS对麻黄碱/假料胺,甲基苯丙胺和1-哌啶环己烷烷腈(PCC)的前体,均为Phenylindine的中间体。一旦检测到残留物,在DEA实验室被收集并在DEA实验室分析使用GC-IRD或质谱法确认疑似物质的疫苗。

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