Poling Process Optimization of Piezo Nano Composite PZT/polimer

摘要

The objective of poling process is to make the electric dipole directions to be parallel in the inside perovskite crystal of piezo materials. In simply way, poling was carried out by giving the two sides of a piezo material by highly electrical potential. More parallel of electrical dipoles, it is more strength the piezo characteristics. The optimization involved control of temperature, time depth and the electrical voltage. The samples was prepared by solgel method with precursor tetrabutyl titanat Ti(OC_4H_9)_4, zirconium nitrat Zr(NO_3)_4.5H_2O, Pb(CH_3COO)_2.3H_2O and solution ethylene glycol. Molar ratio Pb:Zr:Ti = 1,1:0,52:0,48 with concidering lossed Pb. Result of solgel process is nano powder PZT. The formed nano powder PZT was then mixed with polimer PVDF and pressed 10 MPa at 150 °C with the size 15 mm in diameter. After poling, piezoelectric constant d_(33) was measured. The highest d_(33) = 45 pC/N was found at poling parameters V = 5 kV/ mm, T = 120 °C dan time depth = 1 hours.