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Temperature Effects on the Production of Carbon Nanotubes from Palm Oil By Thermal Chemical Vapor Deposition Method

机译:通过热化学气相沉积法从棕榈油生产碳纳米管的温度效应

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In this study we report the effect of various synthesis temperatures of 600 - 1000°C for the synthesis of carbon nanotubes (CNT). Bio-hydrocarbon precursor namely palm oil was utilized as a starting material by thermal vapor deposition method. Ferrocene at 5.33 wt% was directly mixed with palm oil precursor for 30 mins synthesis time. The prepared CNT was collected from the furnace wall and then characterized by field emission scanning electron microscopy, scanning transmission electron microscopy, fourier transform infrared spectroscopy and thermo gravimetric analysis. The density, diameter and the purities of the CNT were found to be highly dependent on the temperature changes. The synthesis temperature of 800°C was considered to be the optimum temperature for higher quality and quantity of CNT production.
机译:在该研究中,我们报告了各种合成温度为600-1000℃的效果,用于合成碳纳米管(CNT)。通过热气相沉积法使用生物 - 烃前体即棕榈油作为原料。二茂铁,5.33wt%与棕榈油前体直接混合30分钟合成时间。从炉壁收集制备的CNT,然后通过现场发射扫描电子显微镜,扫描透射电子显微镜,傅里叶变换红外光谱和热重量分析。发现CNT的密度,直径和纯度高度依赖于温度变化。 800℃的合成温度被认为是高质量和CNT生产量的最佳温度。

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