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Preparation and characterization of thermally expandable microcapsules by in situ polymerization

机译:原位聚合制备和表征可热膨胀的微胶囊

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In the present work, we synthesized microcapsules with copolymer of acrylonitrile and ethyl acrylate as shell and isooctane as core by in situ polymerization, and then optimized the preparative method. Synthesized microcapsules were characterized by Fourier transform infrared spectroscopy (FTIR), ~(13)C nuclear magnetic resonance (~(13)C-NMR), scanning electron microscopy (SEM), particle diameter analysis and thermogravimetry (TG).
机译:在本作工作中,通过原位聚合,我们用丙烯腈和丙烯酸丙烯酸酯和丙烯酸乙酯的共聚物合成微胶囊,然后优化制备方法。通过傅里叶变换红外光谱(FTIR),〜(13)C核磁共振(〜(13)C-NMR),扫描电子显微镜(SEM),粒径分析和热重度(TG),〜(13)C-NMR)。

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