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Preparation and Characterization of LnTaO_4 (Ln = La, Nd, Sm, Dy, Er and Tm)

机译:LNTAO_4的制备和表征(LN = LA,ND,SM,DY,ER和TM)

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Lanthanide tantalite LnTaO_4 (Ln= La, Nd, Sm, Dy, Er and Tm) was synthesized by a solid state reaction between mixed powders of Ln_2O_3 (Ln=La, Nd, Sm, Dy, Er and Tm) and Ta_2O_5. The single-phase LnTaO_4 was prepared by sintering at temperatures of 1423-1673 K in air. The SEM observation showed that the particles were provided with the growth steps and the depeloped facets. The photocatalytic activity for water splitting of LnTaO_4 prepared was measured under UV light irradiation. The activity obtained was higher than that previously reported. These results suggested the crystallinity of LnTaO_4 photocatalysts correlates closely with the efficiency of water splitting.
机译:通过LN_2O_3(LN = La,Nd,Sm,Dy,ER和Tm)和Ta_2O_5的混合粉末之间的固态反应合成镧系元素钽吨LntaO_4(Ln = La,Nd,Sm,Dy,ER和Tm)。通过在空气中的1423-1673k的温度下烧结通过烧结单相LntaO_4。 SEM观察表明,颗粒被提供有生长步骤和已经进孔的刻面。在UV光照射下测量制备的LNTaO_4的水分裂的光催化活性。获得的活性高于先前报道的活性。这些结果表明Lntao_4光催化剂的结晶度与水分裂效率紧密相关。

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