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Synthesis of AgNPs Using Flowers Exhibiting Different Photoresponse

机译:使用呈现不同光响应的花的合成agnps

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Biological synthesis or green synthesis of nanoparticles has proven to be cost effective, rapid and safe. Flowers exhibit different colours due to wavelength selective absorption and light scattering. In this study, four differently coloured flowers, i.e. Bauhinia purpurea — Fabaceae, Couroupita guianensis — Lecithydaceae, Gerbera jamesonii — Asteraceae and Gomphrena globosa — Amaranthaceae were studied for their potency to synthesize silver nanoparticles. The UV-Vis spectrophotometric analysis of the aqueous extracts of B. purpurea, C. guianensis, G. jamesonii and G. globosa flowers recorded their respective peaks at 562, 498, 524 and 548 nm in response to their pigments. The synthesized silver particles were characterized through UV-Vis spectrophotometry, scanning electron microscopy, energy dispersive X-ray spectroscopy, particle size analyzer and fourier transform infrared spectroscopy. The resonance peak in the UV-Vis spectrum was recorded at 430, 420, 445 and 435 nm respectively, for the AgNPs synthesized using B. purpurea, C. guianensis, G. jamesonii and G. globosa. SEM analysis revealed the size range of 107-498 nm for B. purpurea, 15-75 nm for C. guianensis, 17-51 nm for G. jamesonii and 20-91 nm for G. globosa. The presence of silver was confirmed by EDS. The silver particles synthesized using the extracts of B. purpurea, C. guianensis, G. jamesonii and G. globosa showed the average size as 431.3, 71.51, 30.11 and 33.93 nm as assessed through PSA. FTIR studies confirmed the involvement of O-H, N-H, C-C=C, N=0, -N02 and C-O stretches. In the present study, the silver particles synthesized by C. guianensis, G. jamesonii and G. globosa were in the nanoscale, whereas those synthesized by B. purpurea were in microscale. The synthesis of AgNPs is attributed to the pigments or the metabolites present in the floral extracts. Further studies on the potential of flowers exhibiting different photoresponse in the synthesis of nanoparticles are recommended.
机译:生物合成或纳米粒子的绿色合成已被证明具有成本效益,快速,安全。花表现出不同的颜色,由于波长选择吸收和光散射。在这项研究中,四个不同颜色的花朵,即羊蹄甲 - 豆科,Couroupita花草 - Lecithydaceae,非洲菊 - 菊科和千日红 - 苋科研究其效力合成银纳米粒子。 B.菊,C.花草,G.非洲菊以及响应于他们的颜料在562,498,524和548处记录其各自的峰G.藻花的水提取物的紫外 - 可见分光光度分析。通过UV-Vis分光光度法合成的银粒子进行了表征,扫描电子显微镜,能量色散X射线光谱仪,粒度分析仪和傅里叶变换红外光谱。在UV-Vis光谱共振峰在430,420,445和435nm处分别记录,对于使用B.菊,C.花草,G.非洲菊和G.藻合成的AgNPs。 SEM分析显示为B.菊107-498纳米,C.花草15-75纳米,G.非洲菊17-51 nm和G.藻20-91纳米的尺寸范围内。银的存在被证实EDS。使用B.菊,C.花草,G.非洲菊和G.藻的提取物合成的银粒子表现出平均尺寸为431.3,71.51,30.11和33.93处通过PSA评估。 FTIR研究证实-O-H,N-H,C-C = C,N = 0,-NO 2和C-O延伸的参与。在本研究中,由C.花草,G.非洲菊和G.藻中合成的银粒子是纳米级的,而那些由B.菊合成是在微尺度。的AgNPs的合成归因于颜料的或存在于花卉提取物中的代谢物。建议对花朵表现出纳米粒子的合成不同光响应的潜力的进一步研究。

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