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Solvothermal Synthesis of ZnO/CdS Nanocomposite and its Structural and Optical properties

机译:ZnO / Cds纳米复合材料的溶剂热合成及其结构和光学性质

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The Zinc oxide (ZnO) and cadmium sulfide (CdS) nanostructures and ZnO/CdS nanocomposite were prepared by a solvothermal method using acetate precursors using 1:1 volume mixture of water and ethanol as solvent. The structural characterization of the synthesized samples was carried by X-ray diffraction (XRD) technique and the results showed hexagonal and cubic phases for ZnO and CdS, respectively. The surface morphology and elemental compositions were analyzed using FESEM and EDX spectroscopy. The optical absorption and photoluminescence properties were characterized by UV-Visible absorption spectroscopy and photoluminescence spectrometer (PL), respectively. ZnO/CdS nanocomposite shows an enhanced optical absorption with respect to the ZnO and CdS nanostructures. ZnO nanostructures show an intense band edge luminescence.
机译:通过使用乙酸盐前体的溶剂,使用水和乙醇作为溶剂,通过使用乙酸酯前体的溶剂热法制料制备氧化锌(ZnO)和硫化镉(Cds)纳米结构和ZnO / Cds纳米复合材料。合成样品的结构表征由X射线衍射(XRD)技术携带,结果分别显示出ZnO和Cds的六边形和立方相。使用FESEM和EDX光谱分析表面形态和元素组合物。通过UV可见吸收光谱和光致发光光谱仪(PL)的特征在于光学吸收和光致发光性能。 ZnO / Cds纳米复合材料显示出相对于ZnO和Cds纳米结构的增强的光学吸收。 ZnO纳米结构显示强带边缘发光。

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