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Characterization of Diffusion Bonding of Stainless Steel AISI 316 and Pure Titanium sheets Using Copper Interlayer

机译:不锈钢AISI 316和纯钛板的扩散结合表征使用铜层间

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The present work is focused on diffusion bonding between pure titanium and austenitic stainless steel( AISI 316) using interlayer of pure copper foil in vacuum atmosphere of ( 1.5 x10-5 mbr.) at different temperatures (850,900,950 and 990) Co for diffusion times of (20,30,40,50 and 60 min.) under different pressures (1.5,2,3 and 4) Mpa. Many tests and inspections: tensile shear and microhardness tests, also SEM EDS and X-ray diffraction techniques were utilized to characterize the bonded joints. Tensile shear test results showed that the maximum shear strength of diffusion bonded joints was (96.34) MPa at 950oC, pressure 3Mpa and 50 min. with an efficiency of joint (75%) and maximum diffusion depth of (88 μm) The maximum micro hardness of (338.6 Hv )was obtained in the copper interlayer metal compared with the base metals(stainless steel and titanium) due to formations of brittle intermetallic compounds . The EDS and XRD analysis results confirmed the formation of different intermetallic compounds [ FeTi , ( Cu + Ti37Cu63Fex ), TiCu , Ti2Cu, Ti3Cu4 ,] .The surface fracture topography showed that fracture is located at the bright brittle intermetallic compound phase(Ti3Cu4) which was 85% of the fractured area and 15% was at the (Ti2Cu)dark region .
机译:使用在不同温度(850,900,950和990)CO的真空气氛中使用纯铜箔的夹层(850,900,950和990)CO的纯铜箔中的纯铜箔层间的纯铜箔和奥氏体不锈钢(AISI 316)之间的扩散粘合在纯钛和奥氏体不锈钢(AISI 316)之间的扩散键合。 (20,30,40,50和60分钟)在不同压力下(1.5,2,3和4)MPa。许多测试和检查:使用抗拉剪切和显微硬度测试,也使用SEM EDS和X射线衍射技术来表征粘合的关节。拉伸剪切试验结果表明,扩散键合接头的最大剪切强度为950℃,压力3MPa和50分钟的96.34)MPa。具有接头(75%)和(88μm)的最大扩散深度的效率(88μm),与铜层间金属相比,在铜层间金属中获得最大微量硬度(338.6HV),与脆弱的基础金属(不锈钢和钛)相比金属间化合物。 EDS和XRD分析结果证实了不同金属间化合物[FETI,(Cu + Ti37Cu63Fex),TiCu,Ti2Cu,Ti3Cu4]的形成。表面骨折形貌显示断裂位于明亮的脆性金属间化合物相(Ti3Cu4)处是85%的裂缝区域,15%在(Ti2Cu)暗区。

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