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The Effect of Various Acids to the Gelation Process to the Silica Gel Characteristic Using Organic Silica

机译:使用有机二氧化硅将各种酸与硅胶特性凝胶化过程的影响

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Bagasse ash is solid waste of cane sugar industry which contain of silica more than 51%. Some previous study of silica gel from bagasse ash have been conducted often and been applied. This study concerns about the effect of various acid used in the process of gelation to the characteristic of silica gel produced. Then, this silica gel will be used as adsorbent. As that, the silica gel must fulfill the requirements of adsorbent, as have good pores characteristics, fit in mesoporous size so that adsorbent diffusion process is not disturbed. A fitted pores size of silica gel can be prepared by managing acid concentration used. The effect of acid, organic acid (tartaric acid) and inorganic acid (hydrochloric acid), is investigated in detail. The acid is added into sodium silicate solution in that the gel is-formed, the pores structures can be investigated with BET, the crystal form is analyzed with XRD and the pore structure is analyzed visually with SEM. By managing the acid concentration added, it gets the effect of acid to the pore structure of silica gel. The bigger concentration is, the bigger the pore's size of silica gel produced.
机译:Bagasse Ash是蔗糖工业的固体浪费,含有超过51%的硅。已经经常进行并应用来自甘蔗灰灰的硅胶的一些先前研究。本研究涉及各种酸在凝胶化过程中所用的效果,其产生的硅胶的特征。然后,该硅胶将用作吸附剂。如此,硅胶必须满足吸附剂的要求,具有良好的孔特性,适合中孔尺寸,使吸收性扩散过程没有受到干扰。可以通过使用使用的酸浓度来制备硅胶的装配孔尺寸。研究详细研究了酸,有机酸(酒石酸)和无机酸(盐酸)的作用。将酸加入硅酸钠溶液中,使得形成凝胶,孔结构可以用β进行,用XRD分析晶体形式,用SEM直观地分析孔结构。通过管理加入的酸浓度,它使酸与硅胶的孔结构的作用。更大的浓度是,孔隙的硅胶的尺寸越大。

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