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The investigation of changes in properties of composite material containing alumina and stabilized ceria-zirconia solid solution (ACZ) during aging

机译:老化中含氧化铝和稳定的二氧化氮固体溶液(ACZ)的复合材料性能变化的研究

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The study focuses on the development of composite material containing 50 wt. % alumina (Al_2O_3) and 50% mass Ce_(0.4)Zr_(0.5)Y_(0.05)La_(0.05)Ox solid solution by the method of co-precipitation. Also, samples of pure alumina (Al_2O_3) and pure solid solution Ce_(0.4)Zr_(0.5)Y_(0.05)La_(0.05)O_2 were prepared for comparison. Specific surface areas and the pore size distributions were determined by low-temperature adsorption/desorption of nitrogen. Oxide structures were determined by X-ray diffraction. Dynamic of changes in surface areas and crystalline size was investigated. It was shown that the composite has a surface and structure being more thermally stable than the pure composite chemical compound or their mechanical mixture.
机译:该研究侧重于含有50重量%的复合材料的开发。通过共沉淀方法,%氧化铝(Al_2O_3)和50%质量CE_(0.4)Zr_(0.05)γ(0.05)氧化溶液。此外,制备纯氧化铝(Al_2O_3)和纯固溶体Ce_(0.4)Zr_(0.05)y_(0.05)La_2(0.05)O_2的样品进行比较。通过低温吸附/解吸测定氮的比表面积和孔径分布。通过X射线衍射测定氧化物结构。研究了表面积和结晶尺寸的变化的动态。结果表明,复合材料具有比纯复合化学化合物或其机械混合物更热稳定的表面和结构。

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