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Effect of deposition time of sputtering Ag-Cu thin film on mechanical and antimicrobial properties

机译:溅射Ag-Cu薄膜沉积时间对机械和抗微生物性质的影响

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Metallic implants are important components in biomedical treatment. However, post-surgery infection often occurs after installation of implant. The infections are usually treated by antibiotics, but it still causes several secondary problems. As a prevention treatment, the surgical instruments and implants must be in a sterile condition. This action is still not optimal too because the material still can attract the bacteria. From material science point of view, it can be anticipated by developing a type of material which has antibacterial properties or called antimicrobial material. Silver (Ag) and Copper (Cu) have antimicrobial properties to prevent the infection. In this research, the influence of deposition time of Ag-Cu thin film deposition process as antimicrobial material with Physical Vapor Deposition (PVD) RF Sputtering method was analyzed. Deposition time used were for 10, 15 and 20 minutes in Argon gas pressure around 3 × 10~(-2) mbar in during deposition process. The morphology and surface roughness of Ag-Cu thin film were characterized using SEM and AFM. Based on the results, the deposition time influences the quality morphology that the thin films have good homogeneity and complete structure for longer deposition time. In addition, from roughness measurement results show that increase deposition time decrease the roughness of thin film. Antimicrobial performance was analyzed using Kirby Bauer Test. The results show that all of sample have good antimicrobial inhibition. Adhesion quality was evaluated using Rockwell C Indentation Test. However, the results indicate that the Ag-Cu thin film has low adhesion strength.
机译:金属植入物是生物医学治疗中的重要组成部分。然而,手术后感染通常在安装植入后发生。感染通常通过抗生素治疗,但它仍然会导致几个二次问题。作为预防治疗,手术器械和植入物必须处于无菌条件。这种行动仍然不是最佳的,因为材料仍然可以吸引细菌。从材料科学的角度来看,可以通过开发一种具有抗菌性质或称为抗微生物材料的材料来预期。银(Ag)和铜(Cu)具有抗微生物性质以防止感染。在该研究中,分析了Ag-Cu薄膜沉积过程的沉积时间作为具有物理气相沉积(PVD)RF溅射法的抗微生物材料的影响。在沉积过程中,使用的沉积时间为10,15和20分钟,在沉积过程中约为3×10〜(-2)毫巴的氩气压。 Ag-Cu薄膜的形态和表面粗糙度使用SEM和AFM表征。基于该结果,沉积时间影响薄膜具有良好的均匀性和完整结构的质量形态,以便更长的沉积时间。另外,从粗糙度测量结果表明,增加沉积时间降低薄膜的粗糙度。使用Kirby Bauer测试分析了抗微生物性能。结果表明,所有样品都具有良好的抗微生物抑制。使用罗克韦尔C压痕试验评估粘合品质。然而,结果表明Ag-Cu薄膜具有低粘合强度。

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