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Preparation of Novel Magnetic Polyurethane Flexible Foam Nanocomposites

机译:新型磁聚氨酯柔性泡沫纳米复合材料的制备

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Novel magnetic polyurethane flexible foam nanocomposites were synthesized by incorporation of modified magnetic iron oxide nanoparticles into polyure-thane flexible foam. Core shell magnetic nanoparticles (MNPs) Fe3O4@SiO2 were synthesized via co-precipitation and sol-gel methods and incorporated in the structure of the composites by in-situ polymerization of monomers in the presence of MNPs. The magnetic core-shell NPs were used up to 3.0% in the foam formulation and the optimum percentage was defined. The prepared nanocomposites were characterized by scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), vibrating sample magnetometery (VSM), thermo-mechanical analysis (TMA), and thermogravi-metric analysis (TGA). The thermogravimetric analysis results showed an increased thermal stability of the polyurethane flexible foam nanocomposites by incorporation of magnetic core shell nanoparticles.
机译:通过将改性的磁性氧化铁纳米颗粒掺入柔性泡沫中来合成新型磁性聚氨酯柔性泡沫纳米复合材料。通过共沉淀和溶胶 - 凝胶方法合成核壳磁性纳米颗粒(MNP)Fe 3 O 4 @ SiO 2,并通过在MNPS存在下通过原位聚合在复合材料的结构中掺入。磁芯 - 壳NPS在泡沫配方中使用高达3.0%,定义最佳百分比。通过扫描电子显微镜(SEM),傅里叶变换红外光谱(FT-IR),振动样品磁力(VSM),热机械分析(TMA)和热重度分析(TGA),表征制备的纳米复合材料。热重分析结果表明,通过掺入磁芯壳纳米颗粒,可以增加聚氨酯柔性泡沫纳米复合材料的热稳定性。

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