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Influence of Rock Wettability Alteration on Dielectric Dispersion Data

机译:岩石润湿性改变对介电分散数据的影响

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Rock surface wettability controls the fluid distribution in the pore space of the formation and thus, has an influence on its electrical properties. The variation of dielectric dispersion data with the variation of formation wettability is not well understood at present time. In this study, we investigated the influence of wettability alteration on dielectric dispersion data by laboratory experiments using different dielectric data interpretation models. We used a reflection open- ended coaxial probe to measure dielectric dispersion of a 1.5-in. core plug in a frequency range of 10 MHz to 1 GHz. The studied rock wettability was varied in a coreflooding apparatus during a drainage experiment. We used low-polarity oil for the initial drainage to preserve the rock in the water-wet state and added different concentrations of surface-active stearic acid to the oilflood during later drainage stages to change the sample wettability. The used dielectric data interpretation models, in addition to standard interpretation answers, solve for geometrical parameters of the fluids and pore space, which allow us to evaluate wettability variation. Our results showed a decrease in dielectric dispersion at the low-megahertz frequency range as we inject higher acid concentrations into the rock. This decrease in the dispersion also corresponds to an increase of the inverted MN-parameter, which characterizes water phase tortuosity. The results of the inversion, using the textural model, showed a consistent decrease of the depolarization factor of water inclusions as we increase the acid concentration in the injected oil. At the highest acid concentration used (1 wt%), this depolarization factor drops down to 0.36, which is very close to the depolarization factor of spherical inclusions. It follows from our findings that water films, which are characteristic for water-wet rocks, are transformed to more spherical droplets due to the change of wettability to oil-wet state. NMR T2 measurements on the same plug and contact angle measurements on reference samples of same lithology support our conclusions on wettability variation. This study illustrates how to interpret the rock wettability state from dielectric dispersion data based on geometrical models and how to use the inverted geometrical parameters as a wettability indicator.
机译:岩石表面润湿性控制形成的孔隙空间中的流体分布,从而对其电性能产生影响。目前,介电分散数据的变化与形成润湿性的变化并不了解。在这项研究中,我们研究了使用不同介电数据解释模型的实验室实验对润湿性改变对介电分散数据的影响。我们使用了反射开放式同轴探针,以测量1.5英寸的介电分散。核心插头的频率范围为10 MHz至1 GHz。在排水实验期间,研究的岩石润湿性在核心拟合装置中变化。我们使用低极性油用于初始排水,以保持水湿状态的岩石,并在后来的引流阶段期间添加了不同浓度的表面活性硬脂酸,以改变样品润湿性。使用的介电数据解释模型,除了标准解释答案之外,还解决了流体和孔隙空间的几何参数,使我们能够评估润湿性变化。我们的结果表明,当我们将较高的酸浓度注入岩石时,在低兆赫兹频率范围内的介电分散率下降。分散体的这种降低也对应于倒置Mn参数的增加,其表征水相曲折感性。使用纹理模型的反演结果表明,水夹杂物的去极化因子的一致减少,因为我们将注射油中的酸浓度增加。在使用的最高酸浓度(1wt%)中,该去极化因子降至0.36,其非常接近球形夹杂物的去极化因子。它从我们的发现之后,由于对油湿态的润湿性的变化,水膜是水湿岩的特征的特征,这是转变为更球形的液滴。在相同的插头和接触角测量上的NMR T2测量值在相同岩性的参考样本上支持我们对润湿性变化的结论。该研究说明了如何基于几何模型从介电色散数据解释岩石润湿状态,以及如何使用反转的几何参数作为润湿性指示符。

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