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Synthesis of Self-Bonded Pellets of ETS-4 Phase by New Methodology of Preparation

机译:通过制备新方法合成ETS-4相的自粘合颗粒

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We hereby present the results of a research in order to prepare self-bonded pellets of ETS-4 phase by a new methodology of preparation. In particular, the pellets were prepared by kneading crystals of ETS-4 phase and a dry gel, the latter being the precursor for the synthesis of the ETS-4 phase crystals. One of the innovative aspects that is proposed and highlighted in this work is represented by the fact that the dry-gel acts as a "binder". It is characterized by the same chemical composition of crystals, thus avoiding contamination with other elements. In addition, dry-gel allows, the promotion of nucleation phenomena and thus the formation of new crystals of ETS-4 during the pellets baking phases. The pellets were characterized by X-ray diffraction (XRD), Electron microscopy (SEM) and mechanical strength by hardness tester.
机译:我们在此提出了一种研究的结果,以通过新的制备方法制备ETS-4相的自粘合颗粒。特别地,通过捏合ETS-4相和干凝胶的晶体来制备颗粒,后者是合成ETS-4相晶体的前体。在这项工作中提出和突出显示的创新方面之一是由干凝胶作为“粘合剂”的事实表示。它的特征在于晶体的相同化学成分,从而避免与其他元素的污染。此外,干凝胶允许促进成核现象,从而在颗粒烘烤阶段期间形成ETS-4的新晶体。通过硬度测试仪的X射线衍射(XRD),电子显微镜(SEM),电子显微镜(SEM),电子显微镜(SEM)和机械强度的特征在于颗粒。

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