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Preparation and Characterization of Nanostructured CuO Thin Films using Sol-gel Dip Coating

机译:溶胶 - 凝胶浸涂的纳米结构CuO薄膜的制备与表征

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Nanostructured CuO thin films were deposited onto quartz substrates by sol-gel dip coating technique. The precursor solution was prepared by dissolving copper acetate powder into isopropanol with molarity of 0.25M. Preheating and annealing temperature were fixed at 250°C and 600°C respectively. This study focused on various film thicknesses by varying the frequent number of deposited layers. The effect of thickness on electrical, surface morphology and optical properties of CuO thin film were studied. The surface morphology was examined using field emission scanning electron microscopy (FE-SEM), surface profiler for thickness measurement, optical properties of CuO thin film were characterized by using ultraviolet-visible spectroscopy (UV-VIS) for transmittance and absorbance, and the electrical property was examined by using two point probes method. The films were found to be denser at higher film thickness due to lesser porous observed on the surface. The thickness of these CuO thin films varied from 87.14 - 253.58 nm and the direct band gap energy was observed in between 1.9 to 2.35 eV. Lowest resistivity was found for sample with a thickness of 253.58 nm.
机译:通过溶胶 - 凝胶浸涂技术将纳米结构CuO薄膜沉积在石英基板上。通过将醋酸铜粉末溶解到异丙醇中,摩尔溶液为0.25m,通过将乙酸铜粉末溶解在异丙醇中来制备前体溶液。预热和退火温度分别在250℃和600℃下固定。该研究通过改变频繁数量的沉积层来聚焦各种膜厚度。研究了CuO薄膜厚度对电气,表面形态和光学性质的影响。使用场发射扫描电子显微镜(Fe-SEM)检查表面形态,用于厚度测量的表面分析仪,CuO薄膜的光学性质通过使用紫外 - 可见光谱(UV-VI)进行透射率和吸光度,以及电气使用两点探针方法检查性质。由于在表面上观察到较小的多孔,发现薄膜在更高的膜厚度下更密集。这些CuO薄膜的厚度从87.14-253.58nm变化,并且在1.9至2.35eV之间观察到直接带隙能量。发现厚度为253.58nm的样品的最低电阻率。

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