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Preparation of potato starch microfibers obtained by electro wet spinning

机译:通过电湿纺丝获得的马铃薯淀粉微纤维的制备

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Starch is one of the most abundant biopolymer in nature. It has been primarily used as a thickener in the food industry. Starch is found in greater amounts in the potato tubers, which is one of the largest food productions in the region of Boyaca-Colombia. Thus, potatoes are a viable source of starch. The main objective of this study is the preparation and characterization of native starch's microfiber by electro wet-spinning technique. The parameters that were changed for each treatment were as follows: the amount of potential applied to the solution, the distance between the needle and the collector and the rate of injection of the solution in order to determine the physical and chemical properties of the membranes, conformed by potatoes starch microfiber. Diverse instrumental analysis techniques were applied. They were: Scanning Electron Microscopy (SEM) to determine the morphologies and diameters of microfibers, Fourier Transform Infrared Spectroscopy (FTIR) to determine the chemical changes, Thermogravimetric Analysis (TGA) and Differential Calorimetry Scanning (DSC) to obtain the thermal transitions and the temperatures of useful. The microfibers were analysed in order to determine their structural properties and thus define the range of application. In conclusion, potatoes starch microfibers were obtained with average diameters of 15, 17, 23 and 25 micrometres, besides the fibers presented a degradation temperature of 304 °C, indicating that fibers are available with diameters of small scale, with good thermal properties. This study will enable the implementation of the microfibers to obtain bio packaging for food products and other applications.
机译:淀粉是本质上最丰富的生物聚合物之一。它主要用作食品工业中的增稠剂。淀粉在马铃薯块茎中的含量较大,这是Boyaca-哥伦比亚区域最大的食品之一。因此,土豆是一种可行的淀粉来源。本研究的主要目的是通过电湿纺技术制备和表征天然淀粉的微纤维。每种处理改变的参数如下:施加到溶液的电位量,针和收集器之间的距离以及溶液的注射速率,以确定膜的物理和化学性质,由土豆淀粉超细纤维符合。应用不同的仪器分析技术。它们是:扫描电子显微镜(SEM)以确定微纤维的形态和直径,傅里叶变换红外光谱(FTIR)确定化学变化,热重分析(TGA)和差分量热法扫描(DSC)以获得热转换和有用的温度。分析微纤维以确定它们的结构性,从而定义了应用范围。总之,除了纤维呈现为304℃的降解温度的纤维之外,将PotaOS淀粉微纤维得到15,17,23和25微米的淀粉微纤维,表明纤维具有小规模直径的纤维,具有良好的热性能。该研究将能够实现微纤维,以获得用于食品和其他应用的生物包装。

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