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Alcohol sensing properties of SnO_2/CNT nanocomposites synthesized by microwave-assisted process

机译:微波辅助工艺合成的SnO_2 / CNT纳米复合材料的醇感测性能

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SnO_2/CNT nanocomposites were synthesized via microwave-assisted process using SnCl_4-5H_2O as a starting precursor and UV-treated multi-wall carbon nanotubes (MWCNTs) as scaffolds. The concentration of SnCl_4 was varied in the range of 0.01-0.05 M. Effect of precursor concentration on their physical properties and micro structural morphology were investigated by X-ray diffraction (XRD) and scanning electron microscope (SEM). XRD results indicate that the as-synthesized composites are the mixture of two separated phases including SnO_2 and MWCNT. SEM images indicate that the surfaces of MWCNT are thoroughly covered with SnO_2 nanoparticles. Comparative gas sensing result reveals that the prepared hybrid SnO_2/MWCNT composites exhibit much higher sensing sensitivity and recovery property in detecting alcohol gas at room temperature than the bare SnO_2.
机译:通过使用微波辅助工艺合成SnO_2 / CNT纳米复合材料,其使用SnCl_4-5H_2O作为起始前体和UV处理的多壁碳纳米管(MWCNT)作为支架。通过X射线衍射(XRD)和扫描电子显微镜(SEM)研究了SnCl_4的浓度在0.01-0.05m的范围内。通过X射线衍射(XRD)和扫描电子显微镜(SEM)研究了前体浓度对其物理性质和微结构形态的影响。 XRD结果表明,AS合成的复合材料是两个分离阶段的混合物,包括SNO_2和MWCNT。 SEM图像表明MWCNT的表面彻底覆盖有SNO_2纳米颗粒。对比气体感测结果表明,制备的杂交SnO_2 / MWCNT复合材料在比裸SnO_2在室温下检测醇气中的更高感测敏感性和回收性质。

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